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k Report Number 460 QC Report Matrix Spike!Matrix Spike Duplicate Date 11/7/2005 r Project Name Singh Project Number Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 46699-01 <0 50 400 400 41 0 399 ug/L. EPA 8260B 1113105 103 99 9 270 70-130 25 Toluene 46699-01 <0 50 400 400 390 382 ug/L. EPA 82606 1113105 975 95 6 1 99 70-130 25 Tert-Butanol 46699-01 <5 0 200 200 206 221 ug/L EPA 82606 1113105 103 110 692 70-130 25 Methyl-t-Butyl Ether46699-01 57 400 400 56 8 548 ug/L EPA 82608 1113105 128 123 394 70-130 25 Benzene 46699-06 <0 50 400 400 41 8 406 uglL EPA 82608 1112105 104 102 2 91 70-130 25 Toluene 46699-06 <0 50 400 400 405 397 uglL EPA 8260E 1112105 101 992 1 97 70-130 25 Tert-Butanol 46699-06 <50 200 200 240 238 ug/L EPA 8260B 1112105 120 119 0 808 70-130 25 Methyl-t-Butyl Ether 46699-06 <0 50 400 400 404 407 uglL EPA 8260B 1112105 101 102 0 779 70-130 25 Benzene 46719-03 <0 50 400 400 408 401 uglL EPA 8260B 1113105 102 100 1 67 70-130 25 Toluene 46719-03 <0 50 400 400 405 392 uglL EPA 82608 1113105 101 979 343 70-130 25 Tert-Butanol 46719-03 27 200 200 263 262 ug/L. EPA 8260B 1113105 118 118 0 486 70-130 25 Methyl-t-Butyl Ether 46719-03 <0 50 400 400 395 391 uglL EPA 8260B 1113105 98 8 976 1 16 70-130 25 Benzene 46793-05 <0 50 400 400 400 397 uglL EPA 8260B 1115105 99 9 99 2 0 630 70-130 25 Toluene 46793-05 <0 50 400 400 397 394 ug/L EPA 82608 1115105 99 3 984 0 871 70-130 25 Teri-Butanol 46793-05 <5 0 200 200 206 206 ug/L. EPA 82606 11!5105 103 103 0 388 70-130 25 Methyl-t-Butyl Ether 46793-05 290 400 400 323 327 uglL EPA 8260B 1115105 79 8 887 106 70-130 25 I Approved By Joe iff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800 f