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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCalnpbell Analytical 1Tlc Telephone 925-798-1620 Fax 925-798-1622 <br /> I h /lwww mcemVbcll corn E-mail rmm@rwcanVbell corn <br /> Advanced GeoEnvlronmental,Inc Client Project ID Grantline Gas&Food Date Sampled 03/12/03 <br /> 837 Shaw Road I Date Received 03/13/03 <br /> Client Contact Paul Dotson Date Extracted 03/14/03 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 03/14/03 <br /> Oxygenated Volatile Organics by P&T and GC/MS* <br /> ItrM.Ctionmethd SW5030B Analytical Method SW826013 Work Order 0303189 <br /> ILab ID 0303189-OOIC 0303189-002C ! 0303189-003C ! 0303189-0040 <br /> Client ID MWI MW2 MW3 MW4 <br /> iReporting i,tmii for <br /> Matrix W W W W DE—1 <br /> DF 1 1 W 1 1 <br /> 1 S W <br /> i Compound Concentration ug/kg µg/L <br /> iii Dusopropyl ether(DIPE) NO NO NO NO NA 0 5 <br /> IEthyl tert-butyl ether(FTSE) NO ND NO NO NA 0 5 <br /> IMethyl-t-butyl ether(MTBE) 1 5 NO NO NO NA 0 5 <br /> tert-Amyl methyl ether(TAME) NO ND NO NO NA 0 5 <br /> lie <br /> t-Butyl alcohol(TBA) NO NO NO NO NA 50 <br /> Surrogate Recoveries(%) <br /> I %SS 114 119 117 117 <br /> I Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludge/solid samples inµg/kg, wipe samples in lig/wipe, <br /> product/oil/non-aqueous liquid samples in mg/I_ <br /> NO means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> h)fighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> • <br /> DHS Certification No 1644 Angela Rydellus, Lab Manager <br /> I <br />