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110 2nd Avenue South,#137,Pacheco CA 94553-5560 <br /> MCCampbell Analytical Inc Telephone 925-798 1620 Fax 925-798 1622 <br /> h !)www mccampbell corn E-mail ma ca bell com <br /> I _ Advanced GeoEnvironmental, Inc Client Project ID Gran Line Gas&Food Date Sampled 12/19/02 <br /> 837 Shaw Road Date Received 12/20/02 <br />' Client Contact Paul Dotson - Date Extracted 12/23/02-12/24102 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 12123/02-12/24/02 , <br /> IOxygenates and BTEX by GC/MS* <br /> Extraction Method SW503GB Analytical Method SW8260B Work Order 0212368 <br /> ILab ID 0212368-005B 0212368-006B 0212368-0073 <br /> Client ID MW 6 MW 7 MW 8 <br /> Reporting Limit for <br /> Matrix W W { W DF=1 <br /> DF I 1 1 S W <br />' Compound Concentration ugfkg lig/L <br /> ten-Amyl methyl ether(TAME) ND ND ND NA 0 5 <br />' Benzene ND ND ND NA 0 5 <br />' t-Butyl alcohol(TBA) ND ND ND NA 50 <br /> Dusopropyl ether(DIPS) ND ND ND NA 0 5 <br />' Ethylbenzene ND ND ND NA 0 5 <br /> Ethyl tert-butyl ether(ETRE) ND ND ND NA 0 5 <br /> Methyl-t-butyl ether(MTBE) 16 0 88 9 1 NA 0 5 <br />' Toluene ND ND ND NA 0 5 <br /> Xylenes ND ND ND NA 0 5 <br />' Surrogate Recoveries (%) <br /> %SS 986 99 5 987 <br />' Comments i <br /> -T <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludgelsolid samples in pg/kg, wipe samples in pg/wtpe, <br />' product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br />' h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,l)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> 1 <br />