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Sequoia '591D Chmpwalw Drom Redwood City,CA %W3 (4 15) J64-%W FAX(415)344.9]93404 N.Witt Lane Wolaul Crash,CA 945-M <br /> (510) 988-9W FAX(5t0?980.%71 <br /> Analytical 819 Stt;6"M,'ftx,Suite I Sommento,CA s 5834 (914) 921-mm FAX 1916}92 r4iw <br /> U. UlGvron#'V 183 <br /> �Ifol nt oje <br /> UO stonii jililijorngnts <br /> 781 Kingston Ave, Matrix: Wld <br /> Oakland,CA mi i <br /> �Attentlon: Robert Mal,lory 00 Sample Group: 6441944-948 <br /> Reported: may 6, low, <br /> QUALITY CONTROL DATA REPORT <br /> Ana"; TCOMPhIlhone 4-Nitraphencl 2,4-131nitri> Fantwhiorm. Pyrans <br /> folluone phenol <br /> OC 132to#'. SPI34291pa 5PO4$4195 SP042996 SP0429w SP042M <br /> 82MEXA VVOW evom 11270EXA aZFCEXA <br /> ArMlY.Method: FPA 9= EPA BWO EPA 8270 EPA 9270 JEPA82M <br /> Prop.Method: <br /> EPA 3= EPA am EPA3560 EPA35150 EPA3560 <br /> Analyst- ' T.Granicher T.Graniaher T.GranteSer T.GranichBr— T Oraniche-r <br /> MS/MSD iy: 15041672 $041972 6041972 W41an 0041872 <br /> sample conc.: N.D. N.D. N.D. N.D. N,D. <br /> Pre Perod Dete: 4/29/W 4/20/0 4/29/98 4/29/96 4129196 <br /> Analyzed Date. 4/30/98 4/30/96 4/5o/9a 4130/96 4/80/98 <br /> Instrusnent 1.0.#: GC/MS-1 ac/uv IGC/MS-1 GO/M5.1 13c/w1 <br /> Cone.Spiked- gwapoft ISOM 4/kg 2500#g/lQ 000 PUN 2500 pglkg <br /> Result: 2= 2100 law 4900 3400 <br /> MS%He0overy lis 42 se 96 1313 <br /> Dup.Result: 3200 2100 MOO 5900 WOO <br /> MSD%Re cov.: 12a 42 04 118 IGO <br /> RPD; 9.9 CLO 93 22 la <br /> RPD Lim R-. 0050 0-47 0-411 <br /> ,—:42 <br /> Z 01& r.l <br /> LCS I.CgoWins LCSwolft LOS050195 LCSMIQB <br /> Prup2rod oats: $11/90 5/1/96 $/1," ON" 5111W <br /> A=WW Data: 5/2/25 5/1/96 5/2/05 312M S124W <br /> In*UMOM I.D.*: GC/M;3.1 GO/MS-1 OCIMA-1 aq/ms-1 QC/M8.1 <br /> Can&Spiked.- 2500yg/kg 5000paft gbOU pg/kg 5000 polka 25WjugjkU <br /> LC3 Result: 2300 aaw loco 3500 2WO <br /> LOS%Recow 22 BH 70 70 go <br /> US/M31) <br /> LCS 50-140 30-1110 60-1 <br /> Cantirall Umfta <br /> 7r&Mu NM! <br /> Ths LCS is a oontrol aemplo of known,irgerforent4ras matrix that is ana"ed uwng the same MQ*htr,, <br /> preparation,and an*WCW InIftode arnployed*K the samples. The maffl5c`pike is an aliquot of"is <br /> QUOI <br /> A ANALYnCAL.,#1:171 f6ftlFict 011h known quardhies of IlPaCfffo vornpounds and"ooted to the iorittre a"4NqQW procedure. it <br /> T <br /> the f vary of analytes from the matrix spike C10"hat fall Millin specified amntM 11mits Out to fn*k <br /> 77UIC.— int9dOMM,1118 LOS rOCOVVY Is to be wzgd 10 vallcim the hooch, <br /> Kevin Vftn fildrinbrook Mgm Matrix apfige,141190-1143 Durgibato.RPD-AehOm%Differ&nce <br /> Project Mamger Page 2 of 2 <br /> aD41944.rUO <M> <br />