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SAN J O A Q U I , •N Environmental Health Department --COUNTY Complaint Record Daily Time and Activity Summary from6/2V2013 to 6/21/2020 for COLG5PGJR located at BNSF STOCKTON INTERMODAL FACILITY 6540 S AUSTIN RD, STOCKTON Activity Date Recorded by 11/17/2015 3:30 pm: Received the information regarding a possible hazardous materials spill PE 2546 MANZO 90 min at the BNSF intemodal facility. Called James Farrier at 909-267-5167, who SC 544 reported an unconfirmed spill from a small intermodal trailer, the waybill indicates that amine-type chemical was on the truck. 3:50 pm, received a call back from James, he reported that Patriot clean up company will be onsite at 4 pm to unload the trailer and determine the source of the leak. According to the waybill 48-one gallon containers is on the trailer. James reported that the leaked substance looks milky. The trailer is on concrete in the leaker pit area and the trailer was not parked onsite and as far as he knows no spill was onsite and the trailer was brought back to the leak area as soon as the leak was discovered. Called James back, he reported that the estimated ETA is now 5 pm. Jason Neham is onsite at 916-396-0962. The impacted intermodal container No: TTRX##RX360273. Researched the amines, could not find the pH for this substance. According to James, the trailer will be neutralized onsite and the damaged container will be overpacked and sent on to the recipient. Discussed the release with Kasey Foley (Prog. Coordinator), the clean up company can neutralize the chemical at the area of leak and the damaged container should be disposed off as hazardous waste. 11/17/2015 5:00 pm, left to the site. 5:30 pm, arrived onsite, called Jason at 916-396-0962, he PE 2546 MANZO 228 min indicated that he is not onsite and to call Patriot Juan Rubio at 510-829-2198, he SC 944 assisted in locating the"leaker pit". Arrived on scene, took pictures. Observed small whitish drips on the underside of the trailer, looked for the signs of staining, didn't find any, the trailer is on top of plastic, the leaker pit is also lined with plastic with no signs on whitish substance. Took pH of the drips outside of the trailer, with assistance from Juan, pH paper indicated pH between 8 and 9, outside of the container was wet, the reading is likely influenced by the rain water. Provided update to Kasey F. Waited for the trailer to get unloaded. Observed one pallet of corrosive containers(1 gallon), some of which appeared damaged. Discussed the disposal strategy with Juan, absorbent will be applied to all spilled substance inside the trailer, Patriot will unpack the containers any damaged one will be placed into an hazardous waste container along with clean up materials and waste absorbent and left onsite with BNSF for disposal. Twelve (12) damaged 1 gallon containers were recovered and placed into a hazardous waste 55-gallon container which would be staged onsite along with all the clean up materials. The spilled material is a two part epoxy, only one of the parts was damaged, the second part remained intact. Took pictures of the drum and the hazardous waste label. Juan will take a picture of the drum once its moved out of the container and email it to me. He indicated that the outside of the shipping container will be wiped down as well(even though pH was < 12.5) and wipes also placed into the HW drum. The rest of the load was inspected and didn't appear to be damaged and will be repackaged into a new shipping container. Prepared complaint form, entered complaint in ECR, documented the spill response. 8:15 pm, received a page from general hospital From Keith Witkowski (ERTS)440-349-2700 (ext. 307), called Keith and confirmed that the notification was for the same incident and for the same chemical. Finished at 8:48 pm. 11/18/2015 Printed out the complaint, downloaded pictures. PE 2546 MANZO 18 min SC 544 Page 1 of 2