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Sequoia 680 Chesapeake Drive Redwood City CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 404 N Wtget Lane Walnut Creek CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> IIS Analytical 819 Stnkcr Avenue Suite a Sacramento CA 95834 (916) 921 9600 FAX(916)921 Ot00 <br /> Touchstone Developments Client Project ID Chevron 9-4183 /9-4183 <br /> 781 Kingston Matrix Solid <br /> Oakland, CA 94611 <br /> Attention Robert Mallory Work Order# 9604850 01, 02 Reported Apr 25, 1996 <br /> QUALITY CONTROL DATA REPORT <br /> Analyte: Phenol 2-Chlorophenol 1,4-Dichloro N-Nitroso-Dl- <br /> benzene N-propylarnine <br /> QC Batch# MSO415968270EXA MSO415968270EXA MSO415968270EXA MSO415968270EXA <br /> Analy Method EPA 8270 EPA 8270 EPA 8270 EPA 8270 <br /> Prep Method EPA 3550 EPA 3550 EPA 3550 EPA 3550 <br /> Analyst <br /> MS/MSD# <br /> Sample Cone : <br /> Prepared Date <br /> Analyzed Date <br /> Instrument I D # <br /> Cone Spiked <br /> Result <br /> MS% Recovery <br /> Dup Result. <br /> MSD % Recov <br /> RPD <br /> RPD Limit <br /> LCS # SBO41596 SBO41596 SB041596 SB041596 <br /> Prepared Date- 4/15/96 4/15/96 4/15/96 4/15/96 <br /> Analyzed Date 4/15/96 4/15/96 4/15/96 4/15/96 <br /> Instrument I.D # F4 F4 F4 F4 <br /> Cone Spiked 3300 jug/Kg 3300ygft 3300 ug/Kg 3300Jtg/Kg <br /> LCS Result 2500 2800 2400 2500 <br /> LCS %Recov 76 85 73 76 <br /> LCS 35-120 30-120 30-120 30-120 <br /> Control Limits <br /> Please Note <br /> The LCS is a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br /> SEQUOIA ANALYTICAL_ preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch <br /> Kevin Follett **MS=Matrix Spike,MSD=MS Duplicate, RPD=Relative%Difference <br /> Project Manager Page 1 of 3 960485G <3> <br />