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Sequoia 680 Chesapeake Drive Redwood City CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 404 N Wiget Lane Walnut Creek CA 94598 (510) 988 9600 FAX (510) 988 9673 <br /> Analytical 819 Stnker Avenue Suite 8 Sacramento CA 95834 (916) 921 9600 FAX (916)921 0100 <br /> Touchstone Development Client Project ID Chevron 9-4183 <br /> 781 Kingston Matrix Solid <br /> Oakland, CA 94611 <br /> Attention Robert Mallory Work Order# 9604898 06, 07 Reported Apr 23, 1996 <br /> QUALITY CONTROL DATA REPORT <br /> Analyte Phenol 2-Chlorophenol 14-Dichloro N-Nitroso-Di- <br /> benzene N-propylamine <br /> QC Batch# MSO415968270EXA MSO415968270EXA MSO415968270EXA MSO415968270EXA <br /> Analy Method EPA 8270 EPA 8270 EPA 8270 EPA 8270 <br /> Prep Method EPA 3550 EPA 3550 EPA 3550 EPA 3550 <br /> Analyst- <br /> MS/MSD#- <br /> Sample Conc <br /> Prepared Date <br /> Analyzed Date <br /> Instrument I D#. <br /> Conc Spiked <br /> Result <br /> MS % Recovery: <br /> 10 Dup Result <br /> MSD % Recov <br /> RPD <br /> RPD Limit <br /> LCS# SB041596 S6041596 SB041596 SB041596 <br /> Prepared Date 4/15/96 4/15/96 4/15/96 4/15/96 <br /> Analyzed Date 4/15/96 4/15/96 4/15/96 4/15/96 <br /> Instrument I D#- F4 F4 F4 F4 <br /> Conc Spiked 3300 Ng/Kg 3300 pg/Kg 3300 pg/Kg 3300,ug/Kg <br /> LCS Result 2500 2800 2400 2500 <br /> LCS % Recov 76 85 73 76 <br /> LCS 35-120 30-120 30-120 30-120 <br /> Control Limits <br /> Please Note <br /> The LCS is a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br /> WSEQU lA ANALYTICAL preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch <br /> Kevin Follett **MS=Matrix Spike,MSD=MS Duplicate, RPD=Relative%Difference <br /> Project Manager Page 1 of 3 9684898 M <2> <br />