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41� <br /> Sequoia 680 Chesapeake Drive Redwood City CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 404 N Wiget Lane Walnut Creek CA 94598 (510) 988 9,500 FAX(5 10) 988 9673 <br /> 14W Analytical 819 Sinker Avenue Suite 8 Sacramento CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Touchstone Development Client Project ID Chevron 9-4183 <br /> 781 Kingston Matrix Solid <br /> Oakland, CA 94611 <br /> Attention Robert Mallory Work Order# 9604898 06, 07 Reported Apr 23, 1996 <br /> QUALITY CONTROL DATA REPORT <br /> Analyte: 2,4-Dinitro- Pentachloro- Pyrene <br /> toluene phenol <br /> QC Batch# MSO415968270EXA MS0415968270E(A MSO415968270EXA <br /> Analy Method EPA 8270 EPA 8270 EPA 8270 <br /> Prep. Method- EPA 3550 EPA 3550 EPA 3550 <br /> Analyst <br /> MS/MSD#: <br /> Sample Conc . <br /> Prepared Date <br /> Analyzed Date <br /> Instrument I D#: <br /> Conc. Spiked <br /> Result. <br /> MS % Recovery• <br /> Dup Result <br /> MSD % Recov.. <br /> RPD <br /> RPD Limit <br /> LCS# SB041596 SBO41596 SB041596 <br /> Prepared Date 4/15/96 4/15/96 4/15/96 <br /> Analyzed Date: 4/15/96 4/15/96 4/15/96 <br /> Instrument I D # F4 F4 F4 <br /> Conc Spiked 3300Jtg/Kg 3300pg/Kg 3300frg/Kg <br /> LCS Result 2700 2100 2600 <br /> LCS % Recov 82 64 79 <br /> LCS 40-130 30-110 50-115 <br /> Control Limits <br /> Please Note <br /> The LCS is a control sample of known,interferent-free matrix that Is analyzed using the same reagents, <br /> SEQUOIA ANALYTICAL preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> Interference,the LCS recovery Is to be used to validate the batch <br /> K vin Follett MS=Matrix Spike,MSD=MS Duplicate,RPD=Relative%Difference <br /> Project Manager Page 3 of 3 9604898 TTT <4, <br />