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Sequoia 680 Chesapeake Drive Redwood City,CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 15) 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> Iwo Analytical 819 Striker Avenue,Suite 8 Sacramento, CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> }• •n +:Y ` Ah 4'v+.n{ v. .. .. v♦+ r' it r ,r}ivHt W SA+tw}+ <br /> >};Blaine Tech Services, Inc r Client Protect ID Chevron 9-4183/960515-A2r h <br /> 985 Timothy Drive Matrix Liquid r <br /> ,San Jose, CA 95133 <br /> Attention Jim Keller Work Order# 9605C36 -03 Reported May 29,"1,996,' <br /> ^ ,+ <br /> QUALITY CONTROL DATA REPORT <br /> Analyte' Beryllium Cadmium Chromium Nickel <br /> QC Batch#' ME052196601OMDB ME0521966010MDB ME0521966010MDB ME0521966010MDB <br /> Analy. Method. EPA 6010 EPA 6010 EPA 6010 EPA 6010 <br /> Prep. Method' EPA 3010 EPA 3010 EPA 3010 EPA 3010 <br /> Analyst' R Butler R Butler R Butler R Butler <br /> MS/MSD#' 9605BSK1 960585801 960585801 960585801 <br /> Sample Conc . N D N D N D 0 060 <br /> Prepared Date 5/21/96 5/21/96 5/21/96 5/21/96 <br /> Analyzed Date 5/21/96 5/21/96 5/21/96 5/21/96 <br /> Instrument I.D.# MTJA2 MTJA2 MTJA2 MTJA2 <br /> Conc Spiked 10 mg/L 10 mg/L 10 mg/L 10 mg/L <br /> Result 095 094 093 096 <br /> MS %Recovery 95 94 93 90 <br /> Dup. Result 094 093 092 096 <br /> MSD%Recov.. 94 93 92 90 <br /> RPD 10 10 10 00 <br /> RPD Limit 0-20 0-20 0-20 0-20 <br /> LCS# BLK052196 BLK052196 BLK052196 BLK052196 <br /> Prepared Date. 5/21/96 5/21/96 5/21/96 5/21/96 <br /> Analyzed Date. 5/21/96 5/21/96 5/21/96 5/21/96 <br /> Instrument I D.#' MTJA2 MTJA2 MTJA2 MTJA2 <br /> Conc.Spiked. 10 mg/L 10 mg/L 10 mg/L 1 0 mg/L <br /> LCS Result 098 096 095 094 <br /> LCS %Recov ' 98 96 95 94 <br /> IVIS/MSD-- <br /> LCS 80-120 80-120 80-120 80-120 <br /> Control Limits <br /> Please Note <br /> The LCS is a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br /> 10 tecanager <br /> ALYTICAL preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure R <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch <br /> **MS=Matrix Spike,MSD=MS Duplicate,RPD=Relative%Difference 9605C36 BLA 4 1> <br />