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Pace Analytical Services,Inc <br /> 900 Gemrnl Avenue <br /> ace Analytical Houston, 7X 77058 <br /> WWW pacelabs com QUALITY CONTROL DATA Phone 28i 488 i8io <br /> 3 fax 281488 4661 <br /> �r <br /> b T <br /> Lab Project Number 8524929 - <br /> `, Client Project ID BP Site 11191/852 1709 4 <br /> QC Batch 635668 Analysis Method EPA 8260 <br /> QC Batch Method EPAr8260 Analysis Description SW8260 NR Volatiles Soil <br /> Associated Lab Same es 851723714 851723715 851723716 <br /> METHOD B0ANK' 851732247 <br /> Associated Lab Samples 851723714 851723715 851723716 <br /> Blank Reporting <br /> Parameter Units Result Limit Footnotes <br /> Benzene ug/kg ND 5 00 <br /> 1 2-Dibromoethane (EDB) u9/kg ND 5 00 <br /> 1 2-Dichloroethane ug/kg ND 5 00 <br /> Ethylbenzene ug/kg ND 5 00 <br /> Toluene ug/kg ND 5 00 <br /> Xylene (Total) ug/kg ND 5 00 <br /> Methyl tert butyl ether ug/kg ND 5 00 <br /> 2 Methyl-2 propanol ug/kg ND 20 0 <br /> Toluene dB (S) % 98 <br /> 4 Bromofluorobenzene (S) X 97 <br /> 1 2-Dichloroethane d4 (S) X 98 <br /> LABORATORY CONTROL SAMPLE & LCSD 651732248 851732249 <br /> Spike LCS LCSD LCS LCSD <br /> Parameter Units Conc Result Result X Rec X Rec RPD Footnotes <br /> Benzene ug/kg 100 100 7 99 80 101 100 1 <br /> 1 2-Dichloroethane ug/kg 100 106 7 96 77 107 97 10 <br /> Ethylbenzene ug/kg 100 100 7 102 7 101 103 2 <br /> Toluene ug/kg 100 96 47 97 08 96 97 1 <br /> Xylene (Total) ug/kg 300 287 1 289 8 96 97 1 <br /> Methyl-tert-butyl ether ug/kg 100 107 9 90 76 108 91 17 <br /> 2-Methyl-2 propanol ug/kg 500 624 9 374 1 125, 75 50 2 2 <br /> Toluene-d8 (S) 98 98 <br /> 4-Bromofluorobenzene (S) 99 97 <br /> 1 2 Dichloroethane-d4 (S) 104 95 <br /> Date 01/03/02 Page 15 <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced, except in full, <br /> without the written consent of Pace Analytical Services, Inc <br /> M Ace**, <br />