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11 �t II ]� a s A iie. _—un EJ11'i wimncntal Netwoi A WORK ORDER 9710115 QUALITY CONTROL REPORT PAGE QR-5 • ANALYSIS Metals Scan by ICP MATRIX Water LABORATORY CONTROL SAMPLES SAMPLE TYPE Spike Method/Media blank LAB ID IFW_LCS_P INSTR RUN ICP1971015174600/2/1 INSTRUMENT TJA Enviro 36 PREPARED BATCH ID IFW101497 P UNITS mg/L ANALYZED 10/15/97 DILUTION 1 000000 i METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (%) RPD ANALYTE RESULT RESULT LIMIT VALUE (%) LOW HIGH RPD (%) LIMIT (%) Cu Copper 0 124 ND 0 01 0 125 99 2 86 123 Fe Iron 0 529 ND 0 1 0 500 106 84 133 K Potassium 10 0 ND 0 1 10 0 100 80 120 Mg Magnesium 10 3 ND 0 04 10 0 103 80 120 Mn Manganese 0 263 ND 0 005 0 250 105 93 122 Mo Molybdenum 0 198 ND 0 01 0 200 99 0 89 117 Na Sodium 10 3 ND 0 5 10 0 103 80 120 Ni Nickel 0 268 ND 0 01 0 250 107 92 121 Pb Lead 0 529 ND 0 04 0 500 106 90 122 Zn Zinc 0 264 ND 0 01 0 250 106 90 121 LABORATORY CONTROL DUPLICATES SAMPLE TYPE Method Spike Sample Duplicate LAB ID IFW_LCR_P INSTR RUN ICP1971015174600/4/2 INSTRUMENT TJA Enviro 36 PREPARED BATCH ID IFW101497 P UNITS mg/L ANALYZED 10/15/97 DILUTION 1 000000 METHOD REF REPORTING SPIKE RECOVERY REC LIMIT'S (X) RPD . ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (%) Ag Silver 0 0213 0 0216 0 005 1 40 10 Al Aluminum 1 03 1 03 0 1 0 10 Ba Barium 0 998 1 01 0 01 1 20 10 Be Beryllium 0 0242 0 0244 0 002 0 823 10 Ca Calcium 10 1 10 3 0 2 1 96 15 Cd Cadmium 0 0519 0 0522 0 005 0 576 10 Co Cobalt 0 256 0 264 0 005 3 08 10 Cr Chromium 0 101 0 107 0 01 5 77 10 Cu Copper 0 122 0 124 0 01 1 63 10 Fe Iron 0 518 0 529 0 1 2 10 10 K Potassium 9 95 10 0 0 1 0 501 10 Mg Magnesium 10 1 10 3 0 04 1 96 10 Mn Manganese 0 259 0 263 0 005 1 53 10 Mo Molybdenum 0 203 0 198 0 01 2 49 10 Na Sodium 10 2 10 3 0 5 0 976 10 11 Ni Nickel 0 266 0 268 0 01 0 749 10 Pb Lead 0 509 0 529 0 04 3 85 10 Zn Zinc 0 251 0 264 0 01 5 05 10