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• Report Number 40 <br /> QC Report Matrix Spike/Matrix Spike Duplicate Date 5/31/2005 <br /> Project Name Penny Newman Grain <br /> Project Number 050520-KB2 <br /> Duplicate Spiked <br /> Duplicate Spiked Spiked Sample Relative <br /> Spike Spiked Spiked Sample Sample Relative Percent Percent <br /> Spiked Sample Spike pup Sample Sample Analysis Date Percent Percent Percent Recov Diff <br /> Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit <br /> TPH as Diesel Blank <50 1000 1000 931 1020 ug/L M EPA 8015 5/26/05 931 102 903 70-130 25 <br /> Benzene 43917-01 <0 50 400 399 41 6 41 6 ug/L EPA 8260B 5/27105 104 104 0 153 70-130 25 <br /> Toluene 43917-01 <0 50 400 399 41 3 41 1 ug/L EPA 8260B 5127105 103 103 0 272 70-130 25 <br /> Benzene 43926-12 <0 50 39 1 394 41 6 41 7 ug/L EPA 8260B 5127105 106 106 0 559 70-130 25 <br /> Toluene 43926-12 <0 50 39 1 39 4 409 405 ug/L EPA 8260B 5127/05 104 103 1 77 70-130 25 <br /> Benzene 43935-05 <0 50 400 400 38 0 373 ug/L EPA 8260B 5/24105 950 932 1 94 70-130 25 <br /> Toluene 43935-05 <0 50 400 400 382 374 ug/L EPA 8260B 5124105 95 5 934 222 70-130 25 <br /> i <br /> KIFF ANALYTICAL, LLC Approved By Joe iff <br /> 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800 <br />