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1, D — ! Y 4 <br /> Lancaster Laboratories <br /> Where quality is a science. <br /> Page 1 of i <br /> Lancaster Laboratories Sample No. SW 3711720 <br /> Collected: 10/17/2001 09: 40 by EG Account Number: 10869 <br /> Submitted: 10/20/2001 11:00 Chevron Products Company <br /> Reported: 10/31/2001 at 16:58 6001 Bollinger Canyon Rd <br /> Discard: 12/01/2001 Building L, PO Box 6004 j <br /> MW-2-S-40-011017 Grab Soil San Ramon CA 94583-0904 <br /> Facility## 208118 SIRC <br /> 3355 E HammerLn-Stockton NA NA <br /> HL240 <br /> As Received <br /> CAT As Received Method Dilution <br /> No. Analysis Name CAS Number Result Detection Units Factor <br /> Limit <br /> 01725 TPH-GRO N. California (soils) n.a. N.D. 1.0 mg/kg 25 <br /> The reported concentration of TPH-GRO does not include MTBE or other <br /> gasoline constituents eluting prior to the C6 (n-hexane) TPH-GRO range ` <br /> start time. r <br /> The analysis for volatiles was performed on a sample which was preserved <br /> in methanol. The reporting limits were adjusted appropriately. <br /> 02304 UST-Unleaded Soils by 8260B <br /> 02016 Methyl t-butyl ether 1634-04-4 N.D. 1. ug/kg 1 <br /> 05460 Benzene 71-43-2 N.D. 1. ug/kg 1 <br /> 05466 Toluene 108-88-3 N.D. 1_ ug/kg 1 <br /> 05474 Ethylbenzene 100-41-4 N.D. 1. ug/kg 1 <br /> 06301 Xylene (Total) 1330-20-7 N.D. 1. ug/kg 1 <br /> A poor surrogate recovery was observed for the GC/MS volatile fraction. <br /> Theanalysis was repeated and a poor surrogate recovery was again observed <br /> indicating a significant matrix effect. <br /> State of California Lab Certification No_ 2116 <br /> Laboratory Chronicle <br /> CAT Analysis' Dilution <br /> No. Analysis Name Method Trial# Date and,,Time Analyst Factor <br /> 01725 TPH-GRO N. California N. Calif. LUFT 1 10/23/2001 08:44 Martha L. Seidel 25 <br /> (soils) Gasoline method <br /> 02304 UST-Unleaded Soils by SW-846 8260E 1 10/23/2001 16:46 Roy R. Mellott, Jr. 1 <br /> 8260B <br /> 00374 GC/MS VOA Soil Prep SW-846 5030A 1 10/23/2001 14:12 Roy R. Mellott, Jr. n.a. <br /> 01150 GC VOA Soil Prep SW-646 5035 1 10/22/2001 22:36 Martha L. Seidel n.a. <br /> Lancaster Laboratories,Inc. <br /> M E M B E R 2475 New Holland Pike <br /> PO Pax 17.425 <br /> iaiclster,PA 17695-2425 <br /> 717-656-2300 FaK:717-656-2681 2.216 Rev 9/11/00 <br /> i <br /> C <br />