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COLUMBIA ANALYTICAL SERVICES, INC <br /> QA/QC Report <br /> Client (.cmipanv Service Ro-quest S9700532 <br /> Project 21775-206 003/C09193 O 00/)49 S COCK ION Date CuIICLted 3/19/97 <br /> Sample Matrix W,LiLr DateRcceived 3/24/97 <br /> Date Extracted NA <br /> Date Analyzed 3/28/97 <br /> Macri\Spike/Duplicate Matrix Spike Summary <br /> TPH as Gasoline <br /> Sample Nmne MW-; (00) Units ug/L(ppb) <br /> Lab Code 59700532-003MS, S9700532-005DMS Basis NA <br /> Test Notes <br /> Perlent Recovery <br /> CAS Relative <br /> Prep An.ilvsi% Spike Level Sample Spike Result Acceptance Percent <br /> Analyte Method Mc thud MRL MS DMS Result MS DMS MS DMS Limits Difference <br /> Gasoline NONE C.alitornia DHS LUrT 0 5 5000 5000 6200 11000 10 96 -124 75-135 200 <br /> • <br /> DM"20597p <br /> 9700512 XLS Dt"La%41-�" Page 12 Page No <br />