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Sequoia 819 Striker Avenue,Suite:: Sacramento,CA 95834 (916)921-9600 Analytical FAX(916)921-0 t OC IT Corporation-Sacramento Project: Parkinson ARCO Sampled: 1/26/00 1433 N.Market Blvd.,Ste. 1 Project Number: 880-040.1A Received: 1/27/00 Sacramento.CA 95834 Project Manager: Kathleen Waldo Reported: 2/9/00 Volatile Oxygenate Compounds by EPA Method 8260A Sequoia Analytical-Sacramento Batch Date Date Surrogate Reporting Analyte Number Prepared Analyzed Limits Limit Result Units Notes* D-1 10'C S001351-02 Soil Tert-butyl alcohol 0010285 1/31/00 1/31/00 10.0 ND mg/kg Methyl tert-butyl ether " to " 0.100 4.62 " Di-isopropyl ether 11 0.100 ND " Ethyl cert-butyl ether 11 0.100 ND " Tert-amyl methyl ether 11 0.100 0.191 " Ethanol 150 ND " 1,2-Dichloroethane 0.100 ND " Ethylene dibromide 0.100 ND " Surrogate: 1,2-DCA-d4 60.0-140 106 % D-1 10'W 5001351-03 Soil Tert-butyl alcohol 0010285 1/31/00 1/31/00 10.0 ND mg/kg Methyl tert-butyl ether " " " 0.100 3.30 " Di-isopropyl ether " " " 0.100 ND " Ethyl tert-butyl ether 0.100 ND It Tert-amyl methyl ether 0.100 ND " Ethanol " 150 ND 1,2-Dichloroethane 0.100 ND Ethylene dibromide 0.100 ND Surrogate: 1,2-DCA-d4 . 60.0-140 81.6 % D-1 9'N 5001351-04 Soil Tert-butyl alcohol 0010285 1/31/00 1/31/00 10.0 ND mg/kg Methyl tert-butyl ether " " 11 0.100 0.757 " Di-isopropyl ether If " 0.100 ND " Ethyl tert-butyl ether 0.100 ND " Tert-amyl methyl ether 0.100 ND Ethanol 150 ND 1,2-Dichloroethane to 0.100 ND Ethylene dibromide 11 0.100 ND Surrogate: 1,1-DCA-d4 11 60.0-140 78,8 D-1 10'E S001351-05 Soil Tert-butyl alcohol 0010285 1/31/00 1/31/00 10.0 ND mg/kg Methyl tert-butyl ether 11 „ 1. 0.100 2.10 " Di-isopropyl ether 1. 11 to 0.100 ND it Ethyl cert-butyl ether 1. 11 0.100 ND " Tert-amyl methyl ether 11 1. 0.100 ND Ethanol 150 ND " 1,2-Dichloroethane 0.100 ND " Ethylene dibromide 0.100 ND Sequoia Analytical-Sacramento "Refer to end ofreport for text ofnotes and definitions. Page 6 of 16