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1 <br /> CALIFORN,ALaoumySERVICES Environmental <br /> Chemistry <br /> Analyses Report BTEX, EPA Method 602 <br /> Purge and Trap, LPA Method 5030 <br /> Cl2ent Shaw E & 1, Inc. Protect No 8800401A/01060000 <br /> 1326 N. Market Blvd. Contact David Herzog <br /> Sacramento, CA 95834 Phone (916) 565-4367 <br /> Project Parkinson's Arco, Stockton Lab Contact James Liang <br /> Lab ID No U4345 <br /> Date Sampled 01/02/2003 Job No 854345 <br /> Date Recesved 01/02/2003 COC Log No NO NUMBER <br /> Date Extracted N/A Batch No 34166 , <br /> Date Analyzed 01/09/2003 Instrument ID GCO07 <br /> Date Reported 01/14/2003 Analyst ID DAVIDC <br /> Matrix WATER <br /> SURROGATE <br /> Surrogate <br /> Results Surr Conc Recovery Lower Spec Upper Spec , <br /> Analyte CAS No (ug/L) (ug/L) (percent) (Limit) (Limit) <br /> lA / MW-1 <br /> o-Chlorotoluene95498 101 100 101 72 132 ' <br /> 2A / MW-2 <br /> o-Chlorotoluene95498 20 0 20 0 100 72 132 <br /> 3A / MW-3 <br /> o-Chlorotoluene95498 18 9 20 0 95 72 132 <br /> 4A / MW-4 <br /> c-Chlorotoluene95498 19 9 20 0 99 72 132 <br /> 5A / MW-5 <br /> o-Chlorotoluene95498 20 3 20 0 102 72 132 <br /> ANALYTICAL RESULTS <br /> Lab / Client ID Results Rep Limit Dilution <br /> Analyte CAS No (ug/L) (ug/L) (factor) <br /> 1A / MW-1 <br /> Benzene 71432 1000 15 50 <br /> Toluene 108883 44 1 5 5 0 ' <br /> Ethylbenzene 100414 1500 15 50 <br /> Xylenes, total 1330207 310 3 0 5 0 <br /> 2A / MW-2 <br /> Benzene 71432 0 96 0 30 1 0 <br /> Toluene 108883 ND 0 30 1 0 <br /> Ethylbenzene 100414 ND 0 30 1 0 <br /> Xylenes, total 1330207 ND 0 60 1 0 <br /> 3A / MW-3 <br /> Benzene 71432 ND 0 30 1 0 <br /> Toluene 108883 3 8 0 30 1 0 <br /> Ethylbenzene 100414 1 5 0 30 1 0 <br /> Xylenes, total 1330207 2 2 0 60 1 0 <br /> 4A / MW-4 <br /> Benzene 71432 33 0 30 1 0 ' <br /> Toluene 108863 0 73 0 30 1 0 <br /> Ethylbenzene 100414 ND 0 30 1 0 <br /> Xylenes, total 1330207 1 1 0 60 1 0 <br /> 5A / MW-5 , <br /> Benzene 71432 ND 0 30 1 0 <br /> Toluene 108883 0 38 0 30 1 0 <br /> Ethylbenzene 100414 ND 0 30 1 0 <br /> Xylenes, total 1330207 ND 0 60 1 0 <br /> ND = Not detected at or above indicated Reporting Limit <br /> CA DOHS ELAP Accreditation/Regxetration Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 800-638-7301 916-638-7301 Fax- 916-638-4510 <br />