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CALIFORNIA LABORATORY SERVICES <br /> 07/29/05 15 16 <br /> SHAW,E&1 Inc (Sacramento) Project Parkinson's Arco,StocktanCLS Work Order#1 COGO736 <br /> 1326 North Market Blvd Project Number 8800401A <br /> Sacramento CA 95834 Project Manager Dan Wynne <br /> Volatile Organic Compounds by EPA Method 8260E-Quality Control <br /> Reporting Spike Source %P-EC RPD <br /> =A..[�,. Result Li rut Units level Result %REC Linuts RPD Limit Notes <br /> Batch C005531 -EPA 5030 Water MS <br /> Blank(CO0553I-BLK1) Prepared&Analyzed 07122/05 <br /> Di-isopropyl ether ND 050 pg/L <br /> Ethyl tert-butyl ether ND 050 " <br />' Methyl Cert-butyl ether NUJ 050 <br /> tert Amyl methyl ether ND 050 <br /> Tert-butyl alcohol ND 50 <br /> Surrogate Toluene-d8 101 100 101 72-125 <br /> LCS(CO05531-BSl) Prepared&Analyzed 07/22/05 <br /> Methyl tert-butyl ether 225 050 pg/L 200 112 52-130 <br /> *gate Toluene-d8 107 100 107 72-125 <br /> Dap(CO05531-ESDI) _ Prepared&Analyzed 07/22/05 <br /> Methyl Cert-butyl ether 222 050 pg/L 200 Ht t 52-130 1 34 30 <br /> Surrogate Toluene-d8 106 100 106 72-125 <br /> Batch C005551 -EPA 5030 Water MS <br /> Blank(C00555I-BLKI) " Prepared&Analyzed 07/25/05 <br /> Dt-isopropy)ether ND 050 pg/L <br /> Ethyl tert-butyl ether ND 050 <br /> Methyl tert-butyl ether PED 050 <br />' tert-Amyl methyl ether PFD 050 <br /> Tert-butyl alcohol ND 50 <br /> Surrogate Tolue re d8 920 100 920 72-125 <br /> LCS(CO05551-BSI) Prepared&Analyzed 07/25/05 <br /> Methyl ten-butyl ether 203 050 pg/L 200 102 52-130 <br /> Surrogate Toluene-d8 975 100 975 72-125 <br /> t <br /> CA DOHS ELAP Accreditation/Registration Number 1233 <br />' 3249 Fitzgerald Road Rancho Cordova,CA 95742 www.caLfornialab.com 916-638-7301 Fax: 916-638-4510 <br />