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Entech Analytical Labs, Inc. CA FLAP# 2346 <br /> 525 Del Rey Avenue, Suite E • Sunnyvale, CA 94085 + (408) 735-1550 a Fax (408) 735-1554 <br /> ' ATC Associates,Inc. Date: 7/17/00 <br /> 6602 Owens Drive,Suite 100 Date Received: 7/10/00 <br /> ' Pleasanton,CA 94588 <br /> Project Name: <br /> Project Number: 75.625030003/20 <br /> Attn: Jim Lehrman P.O.Number: <br /> Sampled By: Client <br /> ' Certified Analytical Report <br /> Order ID: 21305 Lab Sample ID: 21305-008 Client Sample ID: SB3 <br /> Sample Time: 9:12 AM Sample Date: 7/9/00 Matrix: Solid <br /> Parameter Result Flag DF PQL DLR Units Analysis Date QC Batch ID Method <br /> Diisopropyl Ether ND 1 5 5 µg/Kg 7/14/00 SMS1000714 EPA 8260B <br /> Ethyl-t-butyl Ether ND l 5 5 µg/Kg 7/14/00 SMS1000714 EPA 8260B <br /> (' Methyl-t-butyl Ether ND 1 5 5 pg/Kg 7/14/00 SMS 1000714 EPA 8260B <br /> tert-Amyl Methyl Ether ND 1 5 5 µg/Kg 7/14/00 SMS 1000714 EPA 8260B <br /> tert-Butanol ND 1 20 20 µg/Kg 7/14/00 SMS1000714 EPA 8260B <br /> ' Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Bromofluorobenzene 92 65- 135 <br /> Dibromot7uoromethane 109 65-135 <br /> ' Toluene-d8 102 65-135 <br /> 1 <br /> r' <br /> 1 <br /> =Dilution Factor ND=Not Detected DLR=Detection Limit Reported PQL=Practical Quantitation Limit <br /> Analysis performed by Entech Analytical Labs,Inc.(CA FLAP#2346) <br /> ' Miche , Laboratory Director Environmental Analysis Since 7983 Page 8of9 <br />