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Sequoia680 Chesapeake Dnve Redwood City,CA 94063 (415) 364 9600 FAX (415) 364 9233 <br /> 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> Analytical 8 t 9 Striker Avenue,Suite 8 Sacramento,CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> 'SY..G+gra.w .. ` ,s• -r ' 4.+ c' ..r vG . <br /> Blaine Tech Services, Inc+ Client Project IDr m Chevron 9-1918/960424-A2 <br /> {°985 Timothy Drive Matrix Liquid <br /> ,San Jose, CA 95133 <br /> ,Attention Jim Keller Work Order# 9604192-01-07 Reported May 15, 1996#N <br /> .�tM n{ v!u s {^` vv ir^eMk+ . 4+ nv vuf>�rF rr Ar+ AFrvry vv SvnGii r^}rr. r{n r♦ 'rJ ryGi rvA.'{.r+` 4 � rvr r ryvAG ryr^J r.YfS 'Sry`rh <br /> QUALITY CONTROL DATA REPORT <br /> Analyte: Ortho Phosphate Sulfite Sulfate <br /> GC Batch#: IN043096365200A IN050196377100A IN05149630DOACA <br /> Analy. Method, EPA 365 2 EPA 3771 EPA 300 0 <br /> Prep Method: N/A N/A N/A <br /> Analyst: S Chin D Lawrence S Lee <br /> MS/MSD#: 960419202 9604K4801 960419207 <br /> Sample Conc : 0 086 N D 29 <br /> Prepared Date, 4/30/96 5/1/96 5/14/96 <br /> Analyzed Date. 4/30/96 5/1/96 5/14/96 <br /> Instrument I D#: Manual Manual INIC1 <br /> Conc. Spiked: 0 25 mg/L 10 mg/L 10 mg/L <br /> Result 037 90 40 <br /> MS%Recovery: 114 90 110 <br /> Dup. Result: 037 90 39 <br /> MSD% Recov 114 90 100 <br /> RPD: 00 00 12 <br /> RPD Limit: 0-20 0.20 0-20 <br /> + ♦M'" f r ry r } r r v . .r r ^ V ' v ` ` '�` 4GG' f Gi f vi <br /> tir 11 1Z ti ti55 nnrvv vtirr GG{G+ v vr'r + ry.fM1nG+[+. ryrvr r♦L+ + LA^ + v^ r <br /> LCS#. BLK043096 LCS050196 LCS051496 <br /> Prepared Date: 4/30/96 5/1/96 5/14/96 <br /> Analyzed Date: 4/30/96 5/1/96 5/14/96 <br /> Instrument I D#: Manual Manual INIC1 <br /> Conc. Spiked: 0 25 mg/L 10 mg/L 5 0 mg/L <br /> LCS Result: 025 90 47 <br /> LCS%Recov.: 100 90 94 <br /> 75-125 75-125 75-125 <br /> LCS 80-120 80.120 80`120 <br /> Control Limrts <br /> Please Note <br /> The LCS is a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br /> SE O A ALYTICAL preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> the recovery of analyses from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch <br /> SW <br /> P Manager **MS=Matnx Spike,MSD-MS Duplicate,RPD=Relative%Difference 9604192 BLA <2> <br />