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OVIRONMENTAL <br /> Analytical Chemists <br /> February 15, 2000 ORGANIC Quality Assurance Report for sample(s)STK 30488 1-2 <br /> Spreckles Sugar Co <br /> P o Box 60 Actual sample results are contained in the accompanying analytical report(s) <br /> Tracy, CA 95378 <br /> BATCH EPA CALIBRATION QA/QC METHOD QA/QC <br /> Constituent ID Method Units Type Conic % REC AR NOTE Type Conc % REC % REC AR % DIF MAV NOTE <br /> BFB 0207A219 BTEX EPA ug/L N/A MS 20 00 113 115 61-130 N/A N/A <br /> Benzene 0207A219 BTEX EPA ug/L N/A MS 20 00 100 99 0 70-122 1 0 12 7 <br /> Ethyl Benzene 0207A219 BTEX EPA ug/L N/A M5 20 00 108 111 80-114 2 5 B 1 <br /> Methyl tert-Butyl Ether 0207A219 BTEX EPA ug/L N/A MS 50 00 91 1 88 4 61-140 3 0 20 0 <br /> Toluene 0207A219 BTEX EPA ug/L N/A MS 20 00 107 110 71-120 3 3 24 4 <br /> Xylene 02O7A2i9 BTEX EPA ug/L N/A MS 40 00 110 113 73-124 3 3 10 7 <br /> TPH-Gas 0203A230 EPA 8015 mg/L N/A MS 10 00 99 8 110 75-125 9 6 20 0 <br /> 1,2-Dichloroethane-d4 0209H22A EPA 8260 ug/L CCV 25 0 105 70-130 --- <br /> 0209H22A EPA 8260 ug/L LCS 25 0 106 70-130 MS 25 0 106 111 76-133 4 5 20 0 <br /> Dibromofluromethane 0209H22A EPA 8260 ug/L CCV 25 0 101 78-137 ... <br /> 02091122A EPA 8260 ug/L LCS 25 0 116 78-137 MS 25 0 121 124 76-147 2 2 20 0 <br /> Toluene-68 02091122A EPA 8260 ug/L CCV 25 0 107 82-120 --- <br /> O209H22A EPA 8260 ug/L Les 25 0 98 3 82-120 MS 25 0 95 7 98 6 77-118 2 9 20 0 <br /> 4-Bromofluorobenzene 0209H22A EPA 8260 ug/L CCV 25 0 93 3 83-132 .-- <br /> 0209H22A EPA 8260 ug/L LCS 25 0 110 83-132 MS 25 0 110 108 75-143 1 5 20 0 <br /> N/A => Not Applicable NOTE => See note indicated below <br /> An explanation of QA terms is provided on the reverse side of this page <br /> Notes and comments continued next page . . <br /> I <br /> i u ■u r nrrr ia�.nn. uo..nr—_- <br /> Con2orate Officas&Laboralory Olfice 8 Laboratory Fleld Office <br /> P O Box 272/853 Corporation Street 2500 Stagecoach Road Visalia Cahfomia <br /> Santa Paula CA 93061 0272 Stockton CA 95215 TEL (559)734 9473 <br /> TEL (805)659 0910 TEL (209)942 0181 Mobile (559)737 2399 <br /> FAX (805)525 4172 FAX (209)942 0423 FAX 1559)734 84'15 <br /> `j <br />