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VIRONMENTAL <br /> Analytical Chemists <br /> July 30, 1999 Organic Quality Assurance Report for sample- 932850 <br /> Spreckles Sugar Co Actual sample results are contained in the accompanying analytical report(s) <br /> P O Box 60 <br /> Tracy, CA 95378 <br /> BATCH EPA CALIBRATION GA/QC METHOD QA/QC <br /> Constituent ID Method Units Type Conc X REC AR NOTE Type Conc X REC X REC AR X DIF MAV NOTE <br /> BFB OA219 602 ug/L N/A MS 20 00 108 109 61-130 N/A N/A <br /> Benzene OA219 602 ug/L N/A MS 20 00 98 3 103 70-122 4 3 12 7 <br /> Ethyl Benzene OA219 602 ug/L N/A MS 20 00 98 2 103 80-114 4 4 8 1 <br /> Methyt tert-Butyl Ethe OA219 602 ug/L N/A MS 50 00 72 2 76 7 61-140 5 5 20 0 <br /> Toluene OA219 602 ug/L N/A MS 20 00 94 1 98 2 71-120 4 2 24 4 <br /> xylene OA219 602 ug/L N/A MS 40 00 96 5 100 73-124 4 0 10 7 <br /> 1,2-0lchloroethane-d4 3H22A 8260 ug/L LCS 50 0 97 2 70-130 MS 50 0 102 98 7 76-133 3 4 20 0 <br /> DibromofIuromethane 3H22A 8260 ug/L LCS 50 0 96 9 78-137 MS 50 0 107 101 76-147 5 7 20 0 <br /> Toluene-d8 3H22A 8260 u9/L LCS SO 0 95 1 82-120 MS 50 0 96 8 96 9 77-118 0 1 20 0 <br /> 4-Bromoftuorobenzene 31122A 8260 ug/L LCS 50 0 106 83-132 MS 50 0 102 103 75-143 0 8 20 0 <br /> FGL ID - 19990706 N/A => Not Applicable NOTE a> See note indicated below One or both results S 5*PQL, absolute difference compared. <br /> An explanation of QA terms Is provided on the reverse side of this page <br /> FGL EN IRONMENTAL, INC, <br /> KAD:CL -- <br /> Kurt Wilkinson, B S. , QA Director r <br /> RECEIVE® <br /> UG 0 A 1999 <br /> T.1 Y SUM,? CORPO9rATION <br /> Qo r tomes 8 Lahoratory 0111ce 8 Laboratory Field Office <br /> P O Bon 272/853 Corporation Street 2500 Stagecoach Road Visalia Califomia <br /> Santa Paula CA 93061 0272 Stockton CA 95215 TEL (5S9)734 9473 <br /> TEL (805)659 0910 TEL (209)942 01B1 <br /> Mobile (559)737 2349 <br /> F 1)x (Elfin 5''5 4172 FAX ('wl )312 OI I i rax (',91)17 11 ilI i5 <br />