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�NVIRONMENTAL <br /> Analytical Chemists <br /> December 29, 1998 Organic Quality Assurance Report for sample 836166 <br /> Spreckles Sugar Co Actual sample results are contained in the accompanying analytical report(s) <br /> P 0 Box 60 <br /> Tracy, CA 95378 <br /> BATCH EPA CALIBRATION QA/QC METHOD QA/QC <br /> Constituent ID Method Units Type Cone % REC AR NOTE Type Cone % REC % REC AR % DIF MAV NOTE <br /> 1,2-Dichloroethane-d4 OH22A1 8260 ug/L LCS 50 0 110 70-130 MS 50 0 141 143 76-133 1 5 20 0 411 <br /> Dibromofturomethane OH22A1 8260 ug/L LCS 50 0 90 3 78-137 MS 50 0 103 106 76-147 3 2 20 0 <br /> Toluene-d8 OH22AIi 8260 ug/L LCS 50 0 98 8 82-120 MS 50 0 103 102 77-118 0 6 20 0 <br /> 4-Bromofluorobenzene 0H22A1 8260 ug/L LCS 50 0 100 83-132 MS 50 0 106 105 75-143 0 5 20 0 <br /> Benzene OH22A1 8260 ug/L LCS. 50 0 93 1 68-126 MS 50 0 95 7 96 0 79-123 0 3 20 1 <br /> Chlorobenzene OH22AJ 8260 ug/L LCS 50 0 114 69-136 MS 50 0 103 107 85-122 3 9 14 6 <br /> Chloroform OH22A1 8260 ug/L LCS 50 0 91 8 75-125 MS 50 0 92 6 102 75-125 10 0 20 0 <br /> 1,1-Dichloroethylene OH22A1 8260 ug/L LCS 50 0 83 8 75-125 MS 50 0 85 5 88 4 51-153 3 3 31 2 <br /> Toluene OH22A1 8260 ug/L LCS 50 0 102 75-125 MS 50 0 101 109 86-117 6 9 9 4 <br /> Trichtoroethytene OH22A1 8260 ug/L LCS 50 0 106 65-131 MS 50 0 114 115 62-151 1 2 13 2 <br /> FGL ID = 19981224 N/A => Not Applicable NOTE => See note indicated below <br /> An explanation of QA terms is provided on the reverse side of this page <br /> Notes <br /> 411 Matrix Spike (MS) not within Acceptance Range (AR) . Data was accepted based on the LCS or CCV <br /> recovery <br /> FGL ENVIRONMENTAL, INC. <br /> KAD vt <br /> urt Wilkinson, B S. , QA Director <br /> Coroorale Offices&Laboraloov Office&Laboratory Field Olhce <br /> P O Box 272 1853 Corporation Street 2500 Stagecoach Road Visalia Caldomra <br /> Santa Paula CA 93061 0272 Stockton CA 95215 TEL (209)734 9473 <br /> TEL (805)659 0910 TEL (209)942 0181 Mobile (209)737 2399 <br /> FAX (805)525 4172 FAX (209)942 0423 FAX (209)734 8435 <br /> CA El AP coridir-)liocl Nn 1579 CA El Al"Crrlihr Ilion No 1563 <br /> V <br />