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Report Number 33789 QC Report. Matrix Splkel Matrix Spike Duplicate Date 6/30/2003 Project Name SAN JOAQUIN CATHOLIC Project Number Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Duff Limit Limit Benzene 33799-09 <0 50 400 40 0 409 399 ug/L EPA 8260B 6124103 102 998 233 70-130 25 Toluene 33799-09 <0 50 400 400 434 414 ug/L EPA 8260B 6124103 108 103 4 79 70-130 25 Tert-Butanol 33799-09 <5 0 200 200 197 201 ug/L EPA 8260B 6124103 986 100 2 02 70-130 25 Methyl-t-Butyl Ether 33799-09 <0 50 400 40 0 398 397 ug/L EPA 82608 6124103 996 99 4 0 276 70-130 25 Benzene 33800-01 <0 50 400 400 434 408 uglL EPA 8260B 6/25/03 108 102 617 70-130 25 Toluene 33800-01 <0 50 400 400 421 412 ug/L EPA 8260B 6125/03 105 103 221 70-130 25 Tert-Butanol 33800-01 <5 0 200 200 199 202 ug1L EPA 8260B 6/25/03 994 101 168 70-130 25 Methyl-t-Butyl Ether 33800-01 <0 50 400 400 42 6 440 ug/L EPA 8260B 6125103 106 110 332 70-130 25 Benzene 33789-11 <0 50 400 400 405 391 ug/L EPA 8260E 6124103 101 978 349 70-130 25 Toluene 33789-11 <0 50 400 400 410 394 ug/L EPA 82608 6124/03 102 984 3 91 70-130 25 Tert-Butanol 33789-11 <5 0 200 200 199 193 ug/L EPA 8260B 6124/03 996 967 293 70-130 25 Methyl-t-Butyl Ether33789-11 <0 50 400 400 39 6 391 ug/L EPA 8260B 6/24/03 990 977 135 70-130 25 Benzene 33798-09 <0 50 400 400 419 39 7 ug/L EPA 8260B 6/25/03 105 99 3 527 70-130 25 Toluene 33798-09 <0 50 400 400 420 396 ug/L EPA 8260B 6125103 105 990 593 70-130 25 Tert-Butanol 33798-09 <5 0 200 200 212 204 ug/L EPA 8260B 6/25/03 106 102 362 70-130 25 Methyl-t-Butyl Ether 33798-09 <0 50 400 400 410 395 ug/L EPA 8260B 6/25/03 102 986 375 70-130 25 Approved By J I Kiff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800