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Alpha Analytical, Inc. <br /> 255 Glendale Ave -Suite 21 - Sparks,Nevada 89431-5778 <br /> (775)355-1044 - (775)355-0406 FAX- 1-800-283-1183 <br /> Date <br /> 05-Jan-04 QC Summary Report Work Order <br /> 03122243 <br /> Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID D\MSDCHEM1MS121DATA1031226103122636 D Batch ID MS12W1226C Analysis Date 12/26/2003 21 36 <br /> Sample ID MBLK MS12W1226C Units pg/L Run ID GC/MSD-12_031226B Prep Date 12/26/2003 <br /> Analyte Result POL SpkVal SpkRefVal %REC LowL.imit Highl-imit RPDRefVal %RPD(Limit) Qua] <br /> Tertiary Butyl Alcohol(TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE") ND 05 <br /> Di-isopropyl Ether(DIPE) ND f <br /> Ethvl Tertiary Butyl Ether(ETRE) ND 1 <br /> 1,2-Dichloroethane ND 1 <br /> Benzene ND 05 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 0 5 <br /> 1 2-Dibromoethane (EDB) ND 2 <br /> Ethvibenzene ND 05 <br /> m,p-Xylene ND 05 <br /> o-Xylene ND 05 <br /> Surr 1,2-Dichloroethane-d4 106 10 106 72 126 <br /> Surr Toluene-d6 978 10 98 71 128 <br /> Surr 4-Bromofluorobenzene 909 10 91 76 121 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> Fife ID D1MSDCHEM1MS121DATA1031226103122634 D Batch ID MS12W1226C Analysis Date 12/26/2003 20 54 <br /> Sample ID LCS MS12W1226C Units pg/L Run lD GC/MSD_12_031226B Prep Date 12/26/2003 <br /> Analyte Result POL SpkVal SpkRefVai %REC Lowl-imit HighUmit RPDRefVal %RPD(Limit) Qual <br /> Benzene 103 05 10 103 83 119 <br /> "luene 9 9 05 10 99 80 120 <br /> hylbenzene 101 05 10 101 80 120 <br /> m,p-Xylene 223 05 20 112 77 125 <br /> o-Xylene 103 05 10 103 77 124 <br /> Surr 1,2-Dichloroethane-d4 106 10 108 72 126 <br /> Surr Toluene-d8 101 10 101 71 128 <br /> Surr 4-Bromofluorobenzene 866 10 87 76 121 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D\MSDCHEM1MS121DATA1031226103122637 D Batch ID MS12W1226C Analysis Date 12/26/2003 21 58 <br /> Sample ID 03122243-01AMS Units pg/L Run ID GC/MSD_12_031226B Prep Date 12/26/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowL.imit HighLimit RPDRefVaf %RPD(Limit) Oual <br /> Benzene 491 1 3 50 0 98 59 145 <br /> Toluene 473 1 3 50 0 95 39 161 <br /> Ethylbenzene 471 13 50 0 94 57 145 <br /> m p-Xyiene 105 1 3 100 0 105 37 163 <br /> o-Xylene 48 9 1 3 50 0 98 47 156 <br /> Surr 1,2-Dichloroethane-d4 535 50 107 72 126 <br /> Surr Toluene-d8 493 50 99 71 128 <br /> Surr 4-Bromofluorobenzene 432 50 86 76 121 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW82608 <br /> File ID D\MSDCHEM1MS121DATA1031226103122638 D Batch ID MS12W1226C Analysis Date 12/26/2003 22 19 <br /> Sample ID 03122243-01AMSD Units pg/L Run ID GC/MSD_12_031226B Prep Date 12/26/2003 <br /> Analyte Result POL SpkVal SpkRefVal %REC Lowi-imit Hight-imit RPDRefVal %RPO(Limit) Qua] <br /> Benzene 49 7 1 3 50 0 99 59 145 4911 1 3(22) <br /> Toluene 47 1 3 50 0 94 39 161 4727 0 6(22) <br /> Ethylbenzene 472 1 3 50 0 94 57 145 471 0 1(22) <br /> m,p-Xylene 104 1 3 100 0 104 37 163 1051 0 9(23) <br /> o-Xylene 48 6 1 3 50 0 97 47 156 48 92 0 6(50) <br /> Surr 1,2-Dichloroethane-d4 52 7 50 105 72 126 <br /> ar, <br /> Toluene-d8 489 50 98 71 128 <br /> 4-Bromofluorobenzene 443 50 89 76 121 <br />