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Alpha Analytical, Inc. <br /> + . 255 Glendale Ave •Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044- (775)355-0406 FAX• 1-800-283-1183 <br /> Date Work Order <br /> 03 QC Summary Report W03091741 <br /> Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID D IHPCHEM1MS081DATA1030919103091906 D Batch ID MS8W0919A Analysis Date 09/191200312 19 <br /> Sample ID MBLK MS8W0919A Units pg1L Run ID GCIMSD_8_030919A Prep Date 0911912003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imtt HighLimit RPD Ref Val %RPD Qual <br /> Tertiary Buty]Alcohol(TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 05 <br /> Di-isopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 1 <br /> 1,2-Dichloroethane ND 1 <br /> Benzene ND 0 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 0 5 <br /> 1,2-Dibromoethane(EDB) ND 2 <br /> Ethylbenzene ND 05 <br /> m,p-Xylene ND 05 <br /> o-Xylene ND 0 5 <br /> Surr 1,2-Dichloroethane-d4 988 10 99 72 126 <br /> Surr Toluene-d8 105 10 105 71 128 <br /> Surr 4-Bromofluorobenzene 99 10 99 76 121 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> File ID D}HPCHEMIMS081DATA1030919103091904 D Balch ID MSSW0919A Analysis Date 09/19/2003 11 33 <br /> Sample ID LCS MSBW0919A Units pglL Run ID GC/MSD_8_030919A Prep Date 0911912003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimlt RPD Ref Val %RPD Qual <br /> Benzene 974 0 5 10 97 83 119 <br /> Toluene 976 0 5 10 98 80 120 <br /> Ethylbenzene 10 0 5 10 100 80 120 <br /> m p-Xylene 178 0 5 20 89 77 125 <br /> ylene 889 0 5 10 89 77 124 <br /> r 1,2-Dtchloroethane-d4 973 10 97 72 126 <br /> urr Toluene-d8 101 10 101 71 128 <br /> Surr 4-Bromofluombenzene 975 10 98 76 121 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D 1H PC HEMIMSOMDATAI030919103091909 D Batch ID MS8W0919A Analysis Dale 09/1912003 13 29 <br /> Sample ID 03091741-01AMS Units pg1L Run ID GCIMSD_8_030919A Prep Date 09/1912003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 496 1 3 50 0 99 59 145 <br /> Toluene 48 9 1 3 50 0 98 39 161 <br /> Ethylbenzene 508 1 3 50 0 102 57 145 <br /> m,p-Xylene 886 1 3 900 0 89 37 163 <br /> o-Xylene 451 1 3 50 0 90 47 156 <br /> Surr 1,2-Dichloroethane-d4 51 50 102 72 126 <br /> Surr Toluene-d8 502 50 100 71 128 <br /> Surr 4-Bromofluorobenzene 495 50 99 76 121 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> File ID DIHPCHEMIMS081DATA1030919103091910 D Batch ID MSBW0919A Analysis Date 09/1912003 13 52 <br /> Sample ID 03091741-01AMSD Units pglL Run ID GCIMSD,-8_030919A Prep Date 09119/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLrmit RPD Ref Val %RPD Qual <br /> Benzene 507 1 3 50 0 101 59 145 4961 219 <br /> Toluene 512 1 3 50 0 102 39 161 4894 442 <br /> Ethylbenzene 527 1 3 50 0 105 57 145 5076 383 <br /> m p-xylene 93 1 3 100 0 93 37 163 8861 4 86 <br /> o-Xylene 472 1 3 50 ❑ 94 47 156 451 457 <br /> Surr 1 2-D4chloroethane-d4 492 50 98 72 126 <br /> Surr Toluene-d8 504 50 101 71 128 <br /> Surr 4-Bromofluorobenzene 484 50 97 76 121 <br /> 0 <br />