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Alpha Analytical, Inc. 255 Glendale Ave •Suite 21 • Sparks,Nevada 89431-5778 (775)355-1044• (775)355-0406 FAX• 1-800-283-1183 Wlkte -a4 QC Summary Report Fork Order 0409]744 Method Blank Type MB LK Test Code EPA Method SW8015 File ID Batch ID 10780 Analysis Date 09/21/2004 16 49 Sample ID MBLK-10780 Units pg/L Run ID FID_3_040921A Prep Date 09/21/2004 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual TPH-E (Diesel) ND 50 Surr Nonane 117000 100000 117 40 155 Laboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID Batch ID 10780 Analysis Date 09/21/2004 17 21 Sample ID LCS-10780 Units pg/L Run ID FID 3_040921A Prep Date 09/21/2004 Analyte Result PQL SpkVal SpkRefVal %REC Lowl.imit HighLimit RPDRefVal %RPD(Limit) Qual TPH-E (Diesel) 2470 500 2500 99 57 135 Surr Nonane 119000 100000 119 40 135 Sample Matrix Spike Type MS Test Code EPA Method SW8015 File ID Batch ID 10780 Analysis Date 09/22/2004 04 36 Sample ID 04091704-01AMS Units pg/L Run ID FID 3_040921A Prep Date 09/21/2004 Analyte Result PQL SpkVal SpkRefVal %REC L.owl-imit HighUmd RPDRefVal %RPD(Limit) Qual TPH-E (Diesel) 2520 500 2500 0 101 57 162 Surr Nonane 102000 100000 102 40 155 Sample Matrix Spike Duphcate Type MSD Test Code EPA Method SW8015 File ID Batch ID 10780 Analysis Date 09/22/2004 05 09 Sample ID 04091704-OIAMSD Units pg/L Run ID FID 3 040921A Prep Date 09/21/2004 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighUmit RPDRetVal %RPD(Limit) Qual H-E (Diesel) 2530 500 2500 0 101 57 162 2516 0 6(60) rr Nonane 90900 100000 91 40 155 Comments Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated values may differ shghtly Reported in micrograms per titer,per client request