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1 � <br /> V <br /> Alpha Analytical, Inc. <br /> 255 Glendale Ave - Suite 21 - Sparks,Nevada 89431-5778 6 <br /> (775)355-1044- (775)355-0406 FAX- 1-800-283-1183 <br /> Date <br /> 21-Jun-04 QC Summary Revort Work Order <br /> 04061602 <br /> Method Blank Type MBLK Test Code EPA Method SW8015B/DHS LUFT Manual <br /> File ID D IMSDCHEM1MS121DATA1040616104051605 D Batch ID MS12WO616B Analysis Date 06/16/2004 10 03 <br /> Sample ID MBLK MS12WO616B Units pg/L Run ID MSD_12 040616A Prep Date 06/16/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH Purgeable ND 50 <br /> Surr 1,2-Dichloroethane-d4 971 10 97 72 126 <br /> Surr Toluene-d8 959 10 96 71 128 <br /> Surr 4-Bromofluorobenzene 916 10 92 76 121 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8015B/DHS LUFT Manual <br /> File ID D\MSDCHEM1MS121DATA1040616104061604 D Batch ID MS12W0616B Analysis Date 06/16/2004 09 43 <br /> Sample ID GLCS MS12WO616B Units pg/L Run ID MSD_12 040616A Prep Date 06/16/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH Purqeable 446 50 400 111 67 136 <br /> Surr 1,2-Dichloroethane-d4 10 10 100 72 126 <br /> Surr Toluene-d8 973 10 97 71 128 <br /> Surr 4-Bromofluorobenzene 912 10 91 76 121 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8015B/DHS LOFT Manual <br /> File ID D 1MSDCHEM1MS121DATA1040616104061611 D Batch ID MS12WO616B Analysis Date 06/16/2004 12 12 <br /> Sample ID 04061510-03AGS Units pg/L Run ID MSD 12_040616A Prep Date 06/16/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUmlt HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH Purqeable 2130 250 2000 2244 95 54 154 <br /> Surr 1,2-Dichloroethane-d4 497 50 99 72 126 <br /> rr Toluene-d8 49 50 98 71 126 <br /> rr 4-Bromofluorobenzene 464 50 93 76 121 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW6015B/DHS LUFT Manual <br /> File ID D IMSDCHEM1MS121DATA1040616104061612 D Batch ID MS12WO616B Analysis Date 06/16/2004 12 32 <br /> Sample ID 04061510-03AGSD Units pg/L Run ID MSD_12�040616A Prep Date 06/16/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPM Purqeable 2180 250 2000 2244 98 54 154 2134 2 2(66) <br /> Surr 1,2-Dichloroethane-d4 606 50 101 72 126 <br /> Surr Toluene-d8 485 50 97 71 128 <br /> Surr 4-Bromofluorobenzene 463 50 93 76 121 <br /> Comments <br /> Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated <br /> values may differ slightly <br /> Reported in micrograms per liter,per client request <br />