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Alpha Analytical, Inc. <br /> 255 Glendale Ave • Suite 21 - Sparks,Nevada 89431-5778 <br /> 0 4& (775)355-1044- (775)355-0406 FAX- 1-800-283-1183 <br /> Date <br /> 28-May-04 QC Summary RepWork Order <br /> ort D4051845 <br /> Method Blank Type MBLK Test Code EPA Method SW82608 <br /> File ID D\HPCHEM1MS10\DATA1040519104051932 D Batch ID MS10W0519C Analysis Date 05/19/2004 18 56 <br /> Sample ID MBLK MS10W0519C Units pg/L Run ID MSD_10_040519C Prep Date 05/19/2004 <br /> Analyte Result PQL SpkVai SpkRefVal %REC Lowbmit HighLrmrt RPDRefVal %RPD(L.imd) Qual <br /> Tertiary Butyl Alcohol (TBA) ND 10 <br /> Methyl tert-butyl ether(MTBE) ND 05 <br /> DF-isopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary ButVI Ether(ETRE) ND 1 <br /> 1,2-Dichloroethane ND 1 <br /> Benzene ND 05 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 05 <br /> 1 2-Dibromoethane(EDB) ND 2 <br /> Ethyfbenzene ND 05 <br /> m,p-Xylene ND 05 <br /> o-Xylene ND 05 <br /> Surr 1,2-Dichloroethane-d4 891 10 89 72 126 <br /> Surr Toluene-d8 105 10 105 71 128 <br /> Surr 4-Bromofluorobenzene 996 10 99 6 76 121 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> File ID D\HPCHEM\MS101DATA1040519104051931 D Batch ID MS10W0579C Analysis Date 05/19/20041836 <br /> Sample ID LCS MS10WO519C Units pg/L Run 1D MSD 10 040519C Prep Date 05/19/2004 <br /> Analyte Result PQL SpkVai SpkRefVal %REC Lowl-imit Highijmrt RPDRefVal %RPD(Limit) Qual <br /> Benzene 106 0 5 10 106 83 119 <br /> luene 104 0 5 10 104 80 120 <br /> ylbenzene 105 0 5 10 105 80 120 <br /> Xylene 875 0 5 10 88 77 125 <br /> o-Xylene 8 52 0 5 10 85 77 124 <br /> Surr 1,2-Dichloroethane-d4 95 10 95 72 126 <br /> Surr Toluene-d8 10 10 100 71 128 <br /> Surr 4-Bromofluorobenzene 9 94 10 99 76 121 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> Fife ID D IHPCHEM1MS101DATA1040519104051939 D Batch ID MS10W0519C Analysis Date 05/19/2004 21 22 <br /> Sample ID 04051845-39AMS Units pg/L Run lD MSD 10 040519C Prep Date 05/19/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl unit HighLimit RPORefVal %RPD(Limd) Qual <br /> Benzene 402 1 3 50 0 80 59 145 <br /> Toluene 432 1 3 50 3 6 79 39 161 <br /> Ethyfbenzene 401 13 50 0 80 57 145 <br /> m p-Xylene 34 1 3 50 0 68 37 163 <br /> o-Xylene 339 1 3 50 0 68 47 156 <br /> Surr 1,2-Dichloroethane-d4 497 50 99 72 126 <br /> Surr Toluene-d8 503 50 101 71 128 <br /> Surr 4-Bromofluorobenzene 471 50 94 76 121 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> File lD D\HPCHEM\MS101DATA1040519104051940 D Batch ID MS10W05i9C Analysis Date 05/19/2004 21 43 <br /> Sample ID 04051845-39AMSD Units )tg/L Run lD MSD_10_040519C Prep Date 05/19/2004 <br /> Analyte Result PQL SpkVal SpkRefVaf %REC LowLimit HighLimil RPDRefVal %RPD(Limrt) Qual <br /> Benzene 45 6 1 3 50 0 91 59 145 4017 12 6(22) <br /> Toluene 487 13 50 36 90 39 161 4316 12 1(22) <br /> Ethylbenzene 465 1 3 50 0 93 57 145 401 14 8(22) <br /> m p-XVlene 402 13 50 0 80 37 163 3403 16 5(23) <br /> o-XVlene 393 13 50 0 79 47 156 3387 14 9(50) <br /> Surr 1,2-Dichloroethane-d4 443 50 89 72 126 <br /> Toluene-d8 49 50 98 71 128 <br /> 4-Brom0fluorobenzene 497 50 99 76 121 <br />