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Alpha Analytical, Inc. <br /> 255 Glendale Ave •Suite 21 • Sparks,Nevada 89431-5778 <br /> 4A (775)355-1044• (775)355-0406 FAX• 1-800-283-1183 <br /> Date Work Order <br /> 28-May-04 QC Summary Report W04051845 <br /> Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID C1HPCHEMIMS071DATA1040519104051908 D Batch ID MS07S9941A Analysis Date 05/19/2004 09 58 <br /> Sample ID MBLK MS07S9941A Units pg/Kg Run ID MSD_07_040519A Prep Date 05/19/2004 <br /> Analyte Result PQL SpKVaI SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol (TBA) ND 500 <br /> Methyl tert-butyl ether(MTBE) NO 5 <br /> Di-isopropyl Ether(DIPS) NO 20 <br /> Ethyl Tertiary Butyl Ether(ETRE) NO 20 <br /> 1,2-Dichloroethane ND 20 <br /> Benzene ND 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 20 <br /> Toluene NO 5 <br /> 1,2-Dibromoethane(EDB) NO 40 <br /> Ethylbenzene ND 5 <br /> m,p-Xylene NO 5 <br /> o-Xylene ND 5 <br /> Surr 1,2-Dichloroethane-d4 172 200 86 70 120 <br /> Surr Toluene-d8 200 200 100 79 124 <br /> Surr 4-Bromofluorobenzene 221 200 111 75 122 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> File ID C 1HPCHEMIMS071DATA1040519104os1909 D Batch ID MS07S9941A Analysis Date 05/19/2004 10 20 <br /> Sample ID LCS MS07S9941A Units pg/Kg Run ID MSD 07 040519A Prep Date 05/19/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 221 5 200 110 60 142 <br /> *rpol <br /> uene 217 5 200 108 58 143 <br /> ylbenzene 210 5 200 105 58 147 <br /> -Xylene 217 5 200 109 57 147 <br /> o-Xylene 216 5 200 108 58 149 <br /> Surr 1,2-Dichloroethane-d4 169 200 85 70 120 <br /> Surr Toluene-d8 202 200 101 79 124 <br /> Surr 4-Bromofluorobenzene 215 200 107 75 122 <br /> Sample Matrix Spike Type MS Test Code EPA Method SWO260B <br /> File ID C\HPCHEM\MS071DATA1040519104051911 D Batch ID MS07S9941A Analysis Date 05/19/2004 11 05 <br /> Sample I 04051845-05AMS Units pg/Kg Run ID MSD 07_040519A Prep Date 05/18/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowt-imit HighLimit RPDRefVal %RPD(Lund) Qual <br /> Benzene 168 5 200 0 64 31 152 <br /> Toluene 165 5 200 0 83 11 182 <br /> Ethylbenzene 163 5 200 0 82 30 161 <br /> m,p-Xylene 168 5 200 0 84 0 199 <br /> o-Xylene 165 5 200 0 83 0 208 <br /> Surr 1 2-Dichloroethane-d4 174 200 87 70 120 <br /> Surr Toluene-d8 200 200 100 79 124 <br /> Surr 4-Bromofluorobenzene 214 200 107 75 122 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> File ID C 1HPCHEM1MS071DATA1040519104051912 D Batch 1D MS07SS941A Analysis Date 05/19/2004 11 27 <br /> Sample ID 04051845-OSAMSD Units pg/Kg Run ID MSD_07 040519A Prep Date 05/18/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighUmit RPDRefVal %RPD(Limit) Qual <br /> Benzene 163 5 200 0 81 31 152 1682 3 2(29) <br /> Toluene 162 5 200 0 81 11 182 1661 2 2(44) <br /> Ethylbenzene 160 5 200 0 80 30 161 1634 2 2(29) <br /> m p-Xylene 165 5 200 0 82 0 199 1679 1 9(30) <br /> o-Xylene 160 5 200 0 80 0 208 1654 3 2(30) <br /> Surr 1,2-Dichloroethane-d4 168 200 84 70 120 <br /> r Toluene-d8 202 200 101 79 124 <br /> 4-Bromofluorobenzene 216 200 108 75 122 <br />