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Alpha Analytical, Inc. <br /> 255 GIendale Ave -Suite 21 -Sparks,Nevada 89431-5778 <br /> (775)355-1044- (775)355-0406 FAX - 1-800-283-1183 <br /> ODate <br /> 28 May 04 QC Summary Report Work Order <br /> 04051845 <br /> Method Blank Type MBLK Test Code EPA Method SW02608 <br /> File ID D\HPCHEM1MS091DATA1040519104051940 D Batch 1D MS09SS942A Analysis Date 05/19/2004 22 34 <br /> Sample 1D MBLK MS09S9942A Units pg/Kg Run ID MSD 09 0405196 Prep Date 05/19/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %AEC Lowl-imit HighUmit RPDRetVaf %RPD(Limit) Qual <br /> Tertiary Butvl Alcohol (TBA) ND 500 <br /> Methyl tent-butyl ether(MTBE) ND 5 <br /> 0j-isopropyl Ether(DIPS) ND 20 <br /> Ethyl Tertiary Butyl Ether(ETRE) ND 20 <br /> 1,2-Dichloroethane ND 20 <br /> Benzene ND 5 <br /> Tertiary Amyl Methyf Ether(TAME) ND 20 <br /> Toluene ND 5 <br /> 1 2-Dibromoethane(EDB) ND 40 <br /> Ethylbenzene ND 5 <br /> m,p-Xylene ND 5 <br /> o-Xylene ND 5 <br /> Surr 1,2-Dichloroethane-d4 208 200 104 70 120 <br /> Surr Toluene-d8 196 200 98 79 124 <br /> Surr 4-Bromofluorobenzene 204 200 102 75 122 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> File ID D1HPCHEM1MS091DATA1040519104051941 D Batch 1D MS09S9942A Analysis Date 05/19/2004 22 56 <br /> Sample ID LCS MS09S9942A Units pg/Kg Run ID MSD_09_04051913 Prep Date 05/19/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPDRefVal %RPD(Limit) Qua) <br /> Benzene 224 5 200 112 60 142 <br /> Toluene 222 5 200 111 58 143 <br /> ylbenzene 234 5 200 117 58 147 <br /> IW-Xylene 227 5 200 113 57 147 <br /> o-Xylene 233 5 200 117 58 149 <br /> Surr 1,2-Dichloroethane-d4 211 200 105 70 120 <br /> Surr Toluene-d8 195 200 97 79 124 <br /> Surr 4-Bromofluorobenzene 196 200 98 75 122 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D 1HPCHEM\MS091DATA1040519104051943 D Batch ID MS09S9942A Analysis Date 05/19/2004 23 41 <br /> Sample ID 04051824-01AMS Units pg/Kg Run ID MSD_09 0405198 Prep Date 05/18/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLsmit HighUmit RPDRefVal %RPD(Umit) Quai <br /> Benzene 248 5 200 0 124 31 152 <br /> Toluene 261 5 200 0 130 11 182 <br /> Ethylbenzene 276 5 200 0 138 30 161 <br /> m,p-Xylene 272 5 200 0 136 0 199 <br /> o-Xylene 281 5 200 0 140 0 208 <br /> Surr 1,2-Dichloroethane-d4 204 200 102 70 120 <br /> Surr Toluene-d8 198 200 99 79 124 <br /> Surr 4-Bromofluorobenzene 193 200 96 75 122 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> File ID D\HPCHEM1MS091DATA1040519104051944 D Batch ID MS09S9942A Analysis Date 05/20/2004 00 03 <br /> Sample ID 04051824-01AMSD Units pg/Kg Run ID MSD_09_040519B Prep Date 05/18/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLLmit RPDRefVal %RPD(Limit) Qual <br /> Benzene 226 5 200 0 113 31 152 2484 9 5(29) <br /> Toluene 235 5 200 0 118 11 182 2607 10 3(44) <br /> Ethylbenzene 250 5 200 0 125 30 161 2763 10 2(29) <br /> m,p-Xylene 246 5 200 0 123 0 199 271 7 9 8(30) <br /> o-Xylene 252 5 200 0 126 0 208 2807 10 6(30) <br /> Surr 1 2-Dichloroethane-d4 188 200 94 70 120 <br /> Toluene-d8 197 200 98 79 124 <br /> 4-Brom0fluorobenzene 197 200 98 75 122 <br />