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Alpha Analytical, Inc. <br /> 255 Glendale Ave -Suite 21 - Sparks,Nevada 89431-5778 <br /> 4A (775)355-1044 - (775)355-0406 FAX• 1-800-283-1183 <br /> is Date Work Ord <br /> 28-Mav-04 QC Summary Report er <br /> 04051845 <br /> Method Blank Type MBLK Test Code EPA Method SW826013-DI <br /> File ID C%HPCHEMIMS11\DATA\040526104052603 D Batch ID 10011 Analysts Date 05/26/2004 07 57 <br /> Sample ID MBLK-10011 Units Vg/Kg Run 1D MSD 11_040526A Prep Date 05/26/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowtimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Methanol ND 500 <br /> Ethanol ND 50 <br /> Surr Hexafluoro-2-propanol 464 500 93 69 135 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SWa26013-DI <br /> File ID C IHPCHEMIMS111DATA1040526104052605 D Batch(D 10011 Analysis Date 05/26/2004 08 39 <br /> Sample ID LCS-10011 Units pg/Kg Run ID MSD_11 040526A Prep Date 05/26/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Umit) Qual <br /> Methanol 987 500 1250 79 51 161 <br /> Ethanol 1020 50 1250 82 47 137 <br /> Surr Hexafluoro-2-propanol 452 500 90 69 135 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B-DI <br /> File ID C IHPCHEMIMSt 110ATA1040526104052606 D Batch ID 10011 Analysts Date 05/26/2004 09 00 <br /> Sample ID 04051845-51AMS Units pg/Kg Run ID MSD_11-040526A Prep Date 05/26/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Methanol 1060 500 1250 0 85 51 161 <br /> Ethanol 1000 50 1250 0 80 47 137 <br /> Surr Hexafluoro-2-propanol 454 500 91 69 135 <br /> ample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B-DI <br /> ID C1HPCHEM1MS111DATA1040526104052607 D Batch ID 10011 Analysts Date 05/26/2004 09 21 <br /> mpfe ID 04051845-51AMSD Units pg/Kg Run ID MSD_11 040526A Prep Date 05/26/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighUmtt RPDRefVal %RPD(Limit) Qual <br /> Methanol 931 500 1250 0 74 51 161 1062 13 1(39) <br /> Ethanol 863 50 1250 0 69 47 137 1005 15 2(34) <br /> Surr Hexafluoro-2-propanol 453 500 91 69 135 <br /> Comments <br /> Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated <br /> values may differ slightly <br /> Reported in micrograms per kilogram,per client request <br />