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Alpha Analytical, Inc. <br /> 255 GIendale Ave •Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044• (775)355-0406 FAX• 1-800-283-1183 <br /> Date Work Order <br /> 12-Jur-04 QC Summary Report 04070248 <br /> Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID D 1HPCHEMIMS091DATA1040706104070607 D Batch ID MS09W0706A Analysis Date 07/06/2004 10 51 <br /> Sample ID MBLK MS09W0706A Units pg1L Run ID MSD_09_040706A Prep Date 07!0612004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC L owL imst HrghL:mit RDDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol(TBA) ND 10 <br /> Methyl tert-butyl ether(MTBE) ND 05 <br /> Di-isopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 1 <br /> 1,2-Dichloroethane ND 1 <br /> Benzene ND 05 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 05 <br /> 1,2-Dibromoethane(EDB) ND 2 <br /> Ethylbenzene ND 05 <br /> m,p-Xylene ND 0 5 <br /> o-Xylene ND 05 <br /> Surr 1,2-Dichloroethane-d4 101 10 101 72 126 <br /> Surr Toluene-d8 101 10 101 71 128 <br /> Surr 4-Bromofluorobenzene 945 10 95 76 121 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> File ID D 1HPCHEM%MS091DATA1040706104070605 D Batch ID MS09W0706A Analysis Date 07/06/2004 10 05 <br /> Sample ID LCS MS09W0706A Units jjg1L Run ID MSD_09_040706A Prep Date 07/06/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qua! <br /> Benzene 964 0 5 10 96 83 119 <br /> � <br /> uene 955 0 5 10 96 80 120 <br /> ylbenzene 976 0 5 10 98 80 120 <br /> m p-Xylene 961 0 5 10 96 77 125 <br /> o-Xylene 985 0 5 10 99 77 124 <br /> Surr 1,2-Dichloroethane-d4 105 10 105 72 126 <br /> Surr Toluene-d8 102 10 102 71 128 <br /> Surr 4-Bromofluorobenzene 908 10 91 76 121 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D %HPCHEM1MS091DATA1040706104070608 0 Batch ID MS09W0706A Analysis Date 07/0612004 11 13 <br /> Sample ID 04063030-01AMS Units pg1L Run ID MSD_09_040706A Prep Date 0 710 612 0 04 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imd Hkghl-imit RPDRefVal %RPD(Limit) Qual <br /> Benzene 385 1 3 50 0 77 59 145 <br /> Toluene 373 1 3 50 0 75 39 161 <br /> Ethylbenzene 381 1 3 50 0 76 57 145 <br /> m,p-Xylene 376 1 3 50 0 75 37 163 <br /> o-Xylene 381 13 50 0 76 47 156 <br /> Surr 1,2-Dichloroethane-d4 50 50 100 72 126 <br /> Surr 7oluene-d8 502 50 100 71 128 <br /> Surr 4-Bromofluorobenzene 473 50 95 76 121 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW82608 <br /> File ID D IHPCHEM1MS091DATA1040706104070609 D Batch ID MS09W0706A Analysis Date 07/06/2004 11 35 <br /> Sample ID 04063030-01AMSD Units pg1L Run ID MSD_09_040706A Prep Date 07106/20114 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPDRefVal %RPD(Limit) Qual <br /> Benzene 458 1 3 50 0 92 59 145 3848 17 4(22) <br /> Toluene 449 1 3 50 0 90 39 161 3726 18 6(22) <br /> Ethylbenzene 451 1 3 50 0 90 57 145 3805 16 9(22) <br /> m,p-Xylene 448 1 3 50 0 90 37 163 3759 17 4(23) <br /> o-Xylene 456 1 3 50 0 91 47 156 38 12 17 8(50) <br /> r 1,2-Dichl0roethane-d4 506 50 101 72 126 <br /> Toluene-d8 505 50 101 71 128 <br /> urr 4-Bromofluorobenzene 47 50 94 76 121 <br />