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' Alpha Analytical, Inc. 255 Glendale Ave • Suite 21 • Sparks,Nevada 89431-5778 Oli0& (775)355-1044•(775) 355-0406 FAX • 1-800-283-1183 ate Work Order I8-Mar-04 QC Summar V ReUort 04030847 Method Blank Type MBLK Test Code EPA Method SW8015 File ID Batch ID 9522 Analysis Date 03/09/2004 20 23 Sample ID MBLK 9522 Units pg/L Run ID GC/FID_3_040309A Prep Date 03/09/2004 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-emit HighLimit RPDRefVal %RPD(Limit) Qual TPH-E (Diesel) ND 50 Surr Nonane 86000 100000 86 40 155 Laboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID Batch ID 9522 Analysis Date 03/09/200421 24 Sample ID LCS_9522 Units pg/L Run ID GC/FID_3 040309A Prep Date 03/09/2004 Analyte Result PQL SpkVal SpkReNal %REC LowUmit HighLimit RPDRefVal %RPD(Limit) Qual TPH-E (Diesel) 2440 500 2500 98 57 135 Surr Nonane 75800 100000 76 40 135 Sample Matrix Spike Type MS Test Code EPA Method SW8015 File ID Batch ID 9522 Analysis Date 03/10/2004 18 33 Sample ID 04030847-01AMS Units pg/L Run ID GC/FID 3_040309A Prep Date 03/09/2004 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual TPH-E (Diesel) 2640 500 2500 0 106 57 162 Surr Nonane 100000 100000 100 40 155 Sample Matnx Spike Duplicate Type MSD Test Code EPA Method SW8015 File ID Batch ID 9522 Analysis Date 03/10/2004 19 04 Sample ID 04030847-01AMSO Units p9IL Run ID GC/FID-3-040309A Prep Date 03/09/2004 .abaalyte Result PQL SpkVal SpkRefVal %REC Lowtimit HighLimit RPDRefVal %RPD(Limit) Qual E(Diesel) 2500 500 2500 0 100 57 162 2638 5 2(60) Surr Nonane 92300 100000 92 40 155 Comments Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated values may differ slightly Reported in micrograms per liter,per client request