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COLUMBIA ANALYTICAL SERVICES, INC. <br /> Analytical Report <br /> Client: EMCON Associates Service Request: 5941491 <br /> Project: TOSCO # 1 l 195 /0952-093.02 Date Collected: t 1/18/94 <br /> Sample Matrix: Water Date Received: 11/21/94 <br /> Date Extracted: 11/22/94 <br /> Date Analvzed: 11/24/94 <br /> Hydrocarbon Scan <br /> EPA Method 3510/California DHS LUFC Method <br /> Units: ug/L(ppb) <br /> Mineral TPH as <br /> Analyte: Spirits Jet Fuel Kerosene Diesel Hydraulic Oil <br /> Method Reporting Limit: 50 50 50 50 250 <br /> Sample Name Lab Code <br /> 11195-HPI-W S94149 1-00 1 ND ND ND 370 * 3,000 ** <br /> 11195-HP2-W 5941491-002 ND ND ND ND ND <br /> Method Blank S941122-WB ND ND ND ND ND <br /> * This sample contains components eluting in the diesel range, quantified as diesel. The chromatogram does not <br /> match the typical diesel fingerprint. <br /> - ** This sample contains components clutin <br /> p p gin the hydraulic oil range, quantified as hydraulic oil. The chromatogram <br /> does not match the typical hydraulic oil fingerprint. <br /> Approved By: Date: <br /> 5NU61694 <br />