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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-29703-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-75961 Preparation: 5030B <br /> MS Lab Sample ID: 720-29703-1 Analysis Batch: 720-75961 Instrument ID: HP9 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 08071012.D <br /> Dilution: 5.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 08/07/2010 1531 Final Weight/Volume: 10 mL <br /> Date Prepared: 08/07/2010 1531 <br /> MSD Lab Sample ID: 720-29703-1 Analysis Batch: 720-75961 Instrument ID: HP9 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 08071013.D <br /> Dilution: 5.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 08/07/2010 1604 Final Weight/Volume: 10 mL <br /> Date Prepared: 08/07/2010 1604 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 92 98 60-140 7 20 <br /> 1,1-Dichloroethane 94 102 60-140 8 20 <br /> Dichlorodifluoromethane 82 89 38-140 8 20 <br /> Vinyl chloride 94 103 58-140 9 20 <br /> Chloroethane 106 113 51 -140 6 20 <br /> Trichlorofluoromethane 104 108 60-140 4 20 <br /> Methylene Chloride 90 96 40-140 6 20 <br /> trans-1,2-Dichloroethene 95 103 60-140 8 20 <br /> cis-1,2-Dichloroethene 106 112 60-140 5 20 <br /> Chloroform 95 100 60-140 5 20 <br /> 1,1,1-Trichloroethane 93 101 60-140 8 20 <br /> Carbon tetrachloride 105 113 60-140 7 20 <br /> 1,2-Dichloroethane 102 102 60-140 1 20 <br /> Trichloroethene 93 101 60-140 5 20 <br /> 1,2-Dichloropropane 102 107 60-140 5 20 <br /> Dichlorobromomethane 104 108 60-140 3 20 <br /> trans-1,3-Dichloropropene 107 108 60-140 1 20 <br /> cis-1,3-Dichloropropene 112 115 60-140 2 20 <br /> 1,1,2-Trichloroethane 107 107 60-140 0 20 <br /> Tetrachloroethene 91 96 60-140 6 20 <br /> Chlorodibromomethane 110 111 60-140 1 20 <br /> Chlorobenzene 93 98 60-140 6 20 <br /> Bromoform 107 105 56-140 2 20 <br /> 1,1,2,2-Tetrachloroethane 100 97 60-140 3 20 <br /> 1,3-Dichlorobenzene 96 103 60-140 6 20 <br /> 1,4-Dichlorobenzene 94 100 60-140 6 20 <br /> 1,2-Dichlorobenzene 95 100 60-140 5 20 <br /> Chloromethane 94 102 52-140 8 20 <br /> Bromomethane 107 115 23-140 7 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 91 97 60-140 6 20 <br /> TestAmerica San Francisco Page 49 of 73 <br />