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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-30427-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-77915 Preparation: 5030B <br /> MS Lab Sample ID: 720-30454-A-3 MS Analysis Batch: 720-77915 Instrument ID: HP4 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 091410011.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 09/14/2010 1337 Final Weight/Volume: 10 mL <br /> Date Prepared: 09/14/2010 1337 <br /> MSD Lab Sample ID: 720-30454-A-3 MSD Analysis Batch: 720-77915 Instrument ID: HP4 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 091410012.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 09/14/2010 1409 Final Weight/Volume: 10 mL <br /> Date Prepared: 09/14/2010 1409 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 98 94 60-140 4 20 <br /> 1,1-Dichloroethane 101 99 60-140 1 20 <br /> Dichlorodifluoromethane 74 76 38-140 4 20 <br /> Vinyl chloride 107 109 58-140 2 20 <br /> Chloroethane 102 104 51 -140 2 20 <br /> Trichlorofluoromethane 105 102 60-140 2 20 <br /> Methylene Chloride 103 105 40-140 2 20 <br /> trans-1,2-Dichloroethene 103 101 60-140 2 20 <br /> cis-1,2-Dichloroethene 108 107 60-140 0 20 <br /> Chloroform 99 98 60-140 1 20 <br /> 1,1,1-Trichloroethane 105 102 60-140 3 20 <br /> Carbon tetrachloride 115 110 60-140 4 20 <br /> 1,2-Dichloroethane 99 102 60-140 3 20 <br /> Trichloroethene 104 101 60-140 2 20 <br /> 1,2-Dichloropropane 103 105 60-140 2 20 <br /> Dichlorobromomethane 110 111 60-140 1 20 <br /> trans-1,3-Dichloropropene 111 113 60-140 2 20 <br /> cis-1,3-Dichloropropene 110 111 60-140 1 20 <br /> 1,1,2-Trichloroethane 102 104 60-140 2 20 <br /> Tetrachloroethene 102 99 60-140 3 20 <br /> Chlorodibromomethane 115 118 60-140 2 20 <br /> Chlorobenzene 101 100 60-140 1 20 <br /> Bromoform 110 112 56-140 1 20 <br /> 1,1,2,2-Tetrachloroethane 107 108 60-140 1 20 <br /> 1,3-Dichlorobenzene 103 101 60-140 1 20 <br /> 1,4-Dichlorobenzene 100 99 60-140 1 20 <br /> 1,2-Dichlorobenzene 102 101 60-140 0 20 <br /> Chloromethane 98 101 52-140 2 20 <br /> Bromomethane 99 101 23-140 2 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 100 94 60-140 6 20 <br /> TestAmerica San Francisco Page 14 of 17 <br />