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Client: Environmental Cost Management, Inc. QC Sample Results TestAmerica Job ID: 720-36213-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 8260B -Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: 720-36213-31 MS Client Sample ID: M-10A <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch:95304 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,1,2,2-Tetrachloroethane ND 25.0 27.6 ug/L 110 60-140 <br /> 1,3-Dichlorobenzene ND 25.0 26.5 ug/L 106 60-140 <br /> 1,4-Dichlorobenzene ND 25.0 26.5 ug/L 106 60-140 <br /> 1,2-Dichlorobenzene ND 25.0 26.3 ug/L 105 60-140 <br /> Chloromethane ND 25.0 23.4 ug/L 94 52-140 <br /> Bromomethane ND 25.0 25.8 ug/L 103 23-140 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 25.0 23.0 ug/L 92 60-140 <br /> ne <br /> EDB ND 25.0 29.3 ug/L 117 60-140 <br /> 1,2,4-Trichlorobenzene ND 25.0 25.6 ug/L 102 60-140 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 102 70-130 <br /> 4-Bromofluorobenzene 101 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 100 67-130 <br /> Lab Sample ID: 720-36213-31 MSD Client Sample ID: M-10A <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch:95304 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1-Dichloroethene ND 25.0 22.9 ug/L 92 60-140 1 20 <br /> 1,1-Dichloroethane ND 25.0 25.1 ug/L 100 60-140 0 20 <br /> Dichlorodifluoromethane ND 25.0 20.0 ug/L 80 38-140 4 20 <br /> Vinyl chloride ND 25.0 23.1 ug/L 92 58-140 1 20 <br /> Chloroethane ND 25.0 23.8 ug/L 95 51-140 3 20 <br /> Trichlorofluoromethane ND 25.0 25.6 ug/L 102 60-140 2 20 <br /> Methylene Chloride ND 25.0 23.9 ug/L 96 40-140 0 20 <br /> trans-1,2-Dichloroethene ND 25.0 21.6 ug/L 86 60-140 1 20 <br /> cis-1,2-Dichloroethene 6.9 25.0 36.3 ug/L 118 60-140 0 20 <br /> Chloroform ND 25.0 26.4 ug/L 102 60-140 0 20 <br /> 1,1,1-Trichloroethane ND 25.0 25.2 ug/L 101 60-140 1 20 <br /> Carbon tetrachloride ND 25.0 25.4 ug/L 102 60-140 2 20 <br /> 1,2-Dichloroethane ND 25.0 26.7 ug/L 106 60-140 0 20 <br /> Trichloroethene 210 25.0 212 E 4 ug/L 29 60-140 1 20 <br /> 1,2-Dichloropropane ND 25.0 27.3 ug/L 109 60-140 0 20 <br /> Dichlorobromomethane ND 25.0 31.0 ug/L 124 60-140 0 20 <br /> trans-1,3-Dichloropropene ND 25.0 28.6 ug/L 114 60-140 0 20 <br /> cis-1,3-Dichloropropene ND 25.0 30.2 ug/L 121 60-140 0 20 <br /> 1,1,2-Trichloroethane ND 25.0 28.1 ug/L 112 60-140 1 20 <br /> Tetrachloroethene ND 25.0 24.3 ug/L 97 60-140 2 20 <br /> Chlorodibromomethane ND 25.0 27.6 ug/L 110 60-140 1 20 <br /> Chlorobenzene ND 25.0 26.1 ug/L 104 60-140 1 20 <br /> Bromoform ND 25.0 25.0 ug/L 100 56-140 1 20 <br /> 1,1,2,2-Tetrachloroethane ND 25.0 27.7 ug/L 111 60-140 0 20 <br /> 1,3-Dichlorobenzene ND 25.0 26.3 ug/L 105 60-140 1 20 <br /> 1,4-Dichlorobenzene ND 25.0 26.4 ug/L 106 60-140 0 20 <br /> 1,2-Dichlorobenzene ND 25.0 26.3 ug/L 105 60-140 0 20 <br /> Chloromethane ND 25.0 23.0 ug/L 92 52-140 2 20 <br /> Bromomethane ND 25.0 25.2 ug/L 101 23-140 2 20 <br /> TestAmerica San Francisco <br /> Page 96 of 143 08/16/2011 <br />