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Client: Environmental Cost Management, Inc. QC Sample Results TestAmerica Job ID: 720-36213-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 8260B -Volatile Organic Compounds (GUMS) (Continued) <br /> Lab Sample ID: LCSD 720-95308/7 Client Sample ID: Lab Control Sample Dup <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch:95308 <br /> Spike LCSD LCSD °%Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1-Dichloroethene 25.0 25.1 ug/L 100 64-128 5 20 <br /> 1,1-Dichloroethane 25.0 24.5 ug/L 98 70-130 2 20 <br /> Dichlorodifluoromethane 25.0 19.8 ug/L 79 33-125 3 20 <br /> Vinyl chloride 25.0 25.1 ug/L 100 65-156 6 20 <br /> Chloroethane 25.0 26.3 ug/L 105 62-138 5 20 <br /> Trichlorofluoromethane 25.0 23.3 ug/L 93 72-135 2 20 <br /> Methylene Chloride 25.0 24.9 ug/L 100 73-147 4 20 <br /> trans-1,2-Dichloroethene 25.0 21.9 ug/L 88 68-118 2 20 <br /> cis-1,2-Dichloroethene 25.0 26.8 ug/L 107 70-130 3 20 <br /> Chloroform 25.0 23.2 ug/L 93 70-130 5 20 <br /> 1,1,1-Trichloroethane 25.0 23.7 ug/L 95 70-130 3 20 <br /> Carbon tetrachloride 25.0 24.9 ug/L 100 77-146 5 20 <br /> 1,2-Dichloroethane 25.0 21.8 ug/L 87 70-126 8 20 <br /> Trichloroethene 25.0 24.1 ug/L 96 70-130 0 20 <br /> 1,2-Dichloropropane 25.0 24.6 ug/L 98 70-130 5 20 <br /> Dichlorobromomethane 25.0 24.0 ug/L 96 70-130 8 20 <br /> trans-1,3-Dichloropropene 25.0 23.9 ug/L 96 83-140 10 20 <br /> cis-1,3-Dichloropropene 25.0 23.9 ug/L 96 88-137 8 20 <br /> 1,1,2-Trichloroethane 25.0 24.7 ug/L 99 82-128 9 20 <br /> Tetrachloroethene 25.0 24.3 ug/L 97 70-130 2 20 <br /> Chlorodibromomethane 25.0 24.3 ug/L 97 78-145 10 20 <br /> Chlorobenzene 25.0 25.5 ug/L 102 70-130 1 20 <br /> Bromoform 25.0 25.8 ug/L 103 68-136 5 20 <br /> 1,1,2,2-Tetrachloroethane 25.0 27.3 ug/L 109 70-130 3 20 <br /> 1,3-Dichlorobenzene 25.0 25.5 ug/L 102 70-130 1 20 <br /> 1,4-Dichlorobenzene 25.0 25.1 ug/L 100 87-118 1 20 <br /> 1,2-Dichlorobenzene 25.0 25.0 ug/L 100 70-130 2 20 <br /> Chloromethane 25.0 25.4 ug/L 102 52-175 4 20 <br /> Bromomethane 25.0 26.8 ug/L 107 43-151 3 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 23.7 ug/L 95 42-162 6 20 <br /> ne <br /> EDB 25.0 24.6 ug/L 98 70-130 9 20 <br /> 1,2,4-Trichlorobenzene 25.0 24.8 ug/L 99 70-130 4 20 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 96 70-130 <br /> 4-Bromofluorobenzene 92 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 87 67-130 <br /> Lab Sample ID: 720-36213-13 MS Client Sample ID: M-32D <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch:95308 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,1-Dichloroethene ND 25.0 23.8 ug/L 95 60-140 <br /> 1,1-Dichloroethane ND 25.0 25.0 ug/L 100 60-140 <br /> Dichlorodifluoromethane ND 25.0 18.3 ug/L 73 38-140 <br /> Vinyl chloride ND 25.0 22.9 ug/L 92 58-140 <br /> Chloroethane ND 25.0 24.6 ug/L 98 51-140 <br /> TestAmerica San Francisco <br /> Page 99 of 143 08/16/2011 <br />