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Client: Environmental Cost Management, Inc. QC Sample Results TestAmerica Job ID: 720-36213-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 82608 -Volatile Organic Compounds (GUMS) (Continued) <br /> Lab Sample ID: 720-36213-A-57 MS Client Sample ID: 720-36213-A-57 MS <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch:95330 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 101 70-130 <br /> 4-Bromofluorobenzene 102 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 98 67-130 <br /> Lab Sample ID: 720-36213-A-57 MSD Client Sample ID: 720-36213-A-57 MSD <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch:95330 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1-Dichloroethene ND 25.0 23.4 ug/L 94 60-140 0 20 <br /> 1,1-Dichloroethane ND 25.0 25.6 ug/L 102 60-140 1 20 <br /> Dichlorodifluoromethane ND 25.0 19.2 ug/L 77 38-140 3 20 <br /> Vinyl chloride ND 25.0 22.7 ug/L 91 58-140 1 20 <br /> Chloroethane ND 25.0 23.3 ug/L 93 51-140 2 20 <br /> Trichlorofluoromethane ND 25.0 25.6 ug/L 99 60-140 0 20 <br /> Methylene Chloride ND 25.0 24.2 ug/L 97 40-140 1 20 <br /> trans-1,2-Dichloroethene ND 25.0 22.2 ug/L 89 60-140 2 20 <br /> cis-1,2-Dichloroethene ND 25.0 30.3 ug/L 121 60-140 1 20 <br /> Chloroform ND 25.0 26.0 ug/L 104 60-140 0 20 <br /> 1,1,1-Trichloroethane ND 25.0 25.7 ug/L 103 60-140 0 20 <br /> Carbon tetrachloride ND 25.0 26.2 ug/L 105 60-140 0 20 <br /> 1,2-Dichloroethane ND 25.0 26.7 ug/L 107 60-140 1 20 <br /> Trichloroethene 1.1 25.0 26.2 ug/L 100 60-140 0 20 <br /> 1,2-Dichloropropane ND 25.0 27.1 ug/L 108 60-140 1 20 <br /> Dichlorobromomethane ND 25.0 30.6 ug/L 122 60-140 1 20 <br /> trans-1,3-Dichloropropene ND 25.0 28.8 ug/L 115 60-140 0 20 <br /> cis-1,3-Dichloropropene ND 25.0 30.3 ug/L 121 60-140 0 20 <br /> 1,1,2-Trichloroethane ND 25.0 28.2 ug/L 113 60-140 1 20 <br /> Tetrachloroethene ND 25.0 25.0 ug/L 100 60-140 0 20 <br /> Chlorodibromomethane ND 25.0 27.8 ug/L 111 60-140 0 20 <br /> Chlorobenzene ND 25.0 26.7 ug/L 107 60-140 0 20 <br /> Bromoform ND 25.0 24.8 ug/L 99 56-140 0 20 <br /> 1,1,2,2-Tetrachloroethane ND 25.0 27.3 ug/L 109 60-140 3 20 <br /> 1,3-Dichlorobenzene ND 25.0 26.7 ug/L 107 60-140 0 20 <br /> 1,4-Dichlorobenzene ND 25.0 26.9 ug/L 108 60-140 1 20 <br /> 1,2-Dichlorobenzene ND 25.0 26.6 ug/L 106 60-140 1 20 <br /> Chloromethane ND 25.0 21.9 ug/L 88 52-140 2 20 <br /> Bromomethane ND 25.0 24.7 ug/L 99 23-140 2 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 25.0 23.2 ug/L 93 60-140 0 20 <br /> ne <br /> EDB ND 25.0 28.9 ug/L 116 60-140 1 20 <br /> 1,2,4-Trichlorobenzene ND 25.0 26.0 ug/L 104 60-140 1 20 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 101 70-130 <br /> 4-Bromofluorobenzene 101 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 101 67-130 <br /> TestAmerica San Francisco <br /> Page 105 of 143 08/16/2011 <br />