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Client: Environmental Cost Management, Inc. QC Sample Results TestAmerica Job ID: 720-36213-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 82608 -Volatile Organic Compounds (GUMS) (Continued) <br /> Lab Sample ID: 720-36213-40 MS Client Sample ID:WB-071211 <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch:95331 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,1,2-Trichloroethane ND 25.0 34.0 ug/L 136 60-140 <br /> Tetrachloroethene ND 25.0 23.8 ug/L 95 60-140 <br /> Chlorodibromomethane ND 25.0 32.5 ug/L 130 60-140 <br /> Chlorobenzene ND 25.0 25.6 ug/L 102 60-140 <br /> Bromoform ND 25.0 31.1 ug/L 124 56-140 <br /> 1,1,2,2-Tetrachloroethane ND 25.0 31.1 ug/L 124 60-140 <br /> 1,3-Dichlorobenzene ND 25.0 25.3 ug/L 101 60-140 <br /> 1,4-Dichlorobenzene ND 25.0 25.4 ug/L 102 60-140 <br /> 1,2-Dichlorobenzene ND 25.0 26.1 ug/L 104 60-140 <br /> Chloromethane ND 25.0 21.4 ug/L 86 52-140 <br /> Bromomethane ND 25.0 24.0 ug/L 96 23-140 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 25.0 21.0 ug/L 84 60-140 <br /> ne <br /> EDB ND 25.0 33.9 ug/L 136 60-140 <br /> 1,2,4-Trichlorobenzene ND 25.0 27.5 ug/L 110 60-140 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits u <br /> Toluene-d8(Surr) 100 70-130 <br /> 4-Bromofluorobenzene 98 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 112 67-130 <br /> Lab Sample ID: 720-36213-40 MSD Client Sample ID:WB-071211 <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch:95331 <br /> Sample Sample Spike MSD MSD °%Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1-Dichloroethene ND 25.0 20.1 ug/L 80 60-140 12 20 <br /> 1,1-Dichloroethane ND 25.0 24.0 ug/L 96 60-140 7 20 <br /> Dichlorodifluoromethane ND 25.0 13.6 ug/L 54 38-140 14 20 <br /> Vinyl chloride ND 25.0 18.9 ug/L 76 58-140 5 20 <br /> Chloroethane ND 25.0 21.8 ug/L 87 51-140 4 20 <br /> Trichlorofluoromethane ND 25.0 17.3 ug/L 69 60-140 12 20 <br /> Methylene Chloride ND 25.0 27.5 ug/L 110 40-140 4 20 <br /> trans-1,2-Dichloroethene ND 25.0 20.0 ug/L 80 60-140 7 20 <br /> cis-1,2-Dichloroethene ND 25.0 27.9 ug/L 111 60-140 5 20 <br /> Chloroform ND 25.0 24.3 ug/L 97 60-140 4 20 <br /> 1,1,1-Trichloroethane ND 25.0 19.7 ug/L 79 60-140 12 20 <br /> Carbon tetrachloride ND 25.0 19.7 ug/L 79 60-140 14 20 <br /> 1,2-Dichloroethane ND 25.0 27.6 ug/L 110 60-140 3 20 <br /> Trichloroethene ND 25.0 22.4 ug/L 90 60-140 8 20 <br /> 1,2-Dichloropropane ND 25.0 28.6 ug/L 114 60-140 3 20 <br /> Dichlorobromomethane ND 25.0 28.6 ug/L 114 60-140 3 20 <br /> trans-1,3-Dichloropropene ND 25.0 31.5 ug/L 126 60-140 1 20 <br /> cis-1,3-Dichloropropene ND 25.0 29.5 ug/L 118 60-140 2 20 <br /> 1,1,2-Trichloroethane ND 25.0 33.5 ug/L 134 60-140 1 20 <br /> Tetrachloroethene ND 25.0 21.6 ug/L 86 60-140 10 20 <br /> Chlorodibromomethane ND 25.0 32.2 ug/L 129 60-140 1 20 <br /> Chlorobenzene ND 25.0 25.2 ug/L 101 60-140 2 20 <br /> Bromoform ND 25.0 31.8 ug/L 127 56-140 2 20 <br /> 1,1,2,2-Tetrachloroethane ND 25.0 31.3 ug/L 125 60-140 1 20 <br /> TestAmerica San Francisco <br /> Page 109 of 143 08/16/2011 <br />