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Client: Environmental Cost Management, Inc. QC Sample Results TestAmerica Job ID: 720-36472-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 8260B -Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCSD 720-96122/21 Client Sample ID: Lab Control Sample Dup <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch:96122 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,2-Dichloroethane 25.0 23.7 ug/L 95 70-126 0 20 <br /> Trichloroethene 25.0 23.8 ug/L 95 70-130 0 20 <br /> 1,2-Dichloropropane 25.0 26.9 ug/L 108 70-130 1 20 <br /> Dichlorobromomethane 25.0 26.5 ug/L 106 70-130 1 20 <br /> trans-1,3-Dichloropropene 25.0 28.5 ug/L 114 83-140 1 20 <br /> cis-1,3-Dichloropropene 25.0 28.1 ug/L 112 88.137 0 20 <br /> 1,1,2-Trichloroethane 25.0 27.6 ug/L 110 82-128 2 20 <br /> Tetrachloroethene 25.0 23.1 ug/L 92 70-130 0 20 <br /> Chlorodibromomethane 25.0 27.5 ug/L 110 78-145 0 20 <br /> Chlorobenzene 25.0 24.9 ug/L 100 70-130 0 20 <br /> Bromoform 25.0 27.3 ug/L 109 68-136 1 20 <br /> 1,1,2,2-Tetrachloroethane 25.0 28.0 ug/L 112 70-130 0 20 <br /> 1,3-Dichlorobenzene 25.0 25.3 ug/L 101 70-130 1 20 <br /> 1,4-Dichlorobenzene 25.0 25.0 ug/L 100 87-118 2 20 <br /> 1,2-Dichlorobenzene 25.0 25.5 ug/L 102 70-130 2 20 <br /> Chloromethane 25.0 17.6 ug/L 70 52-175 6 20 <br /> Bromomethane 25.0 17.5 ug/L 70 43-151 6 20 El <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 22.8 ug/L 91 42-162 4 20 <br /> ne <br /> EDB 25.0 27.4 ug/L 110 70-130 1 20 <br /> 1,2,4-Trichlorobenzene 25.0 26.0 ug/L 104 70-130 4 20 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 96 70-130 <br /> 4-Bromofluorobenzene 100 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 94 67-130 <br /> Method: EPA 524.2 - PURGEABLE ORGANIC COMPOUNDS BY GC/MS (EPA 524.2) <br /> Lab Sample ID: 11G3546-BLK1 Client Sample ID: Method Blank <br /> Matrix:Water Prep Type:Total <br /> Analysis Batch: 11G3546 Prep Batch: 11133546P <br /> Blank Blank <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Bromodichloromethane ND 0.10 ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> Bromoform ND 0.10 ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> Bromomethane ND 2.5 ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> Carbon tetrachloride ND 0.10 ug/I 07/29/11 08:07 07/29/11 09:00 1.00 <br /> Chlorobenzene ND 0.10 ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> Chloroethane ND 0.10 ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> Chloroform ND 0.10 Ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> Chloromethane ND 0.50 Ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> Dibromochloromethane ND 0.10 Ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> 1,2-Dibromoethane(EDB) ND 0.10 ug/I 07/29/11 08:07 07/29/11 09:00 1.00 <br /> 1,2-Dichlorobenzene ND 0.10 ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> 1,3-Dichlorobenzene ND 0.10 ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> 1,4-Dichlorobenzene ND 0.10 ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> 1,1-Dichloroethane ND 0.10 ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> 1,2-Dichloroethane ND 0.10 ug/I 07/29/1108:07 07/29/1109:00 1.00 <br /> TestAmerica San Francisco <br /> Page 14 of 35 08/05/2011 <br />