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Client: Environmental Cost Management, Inc. Quality Control Data TestAmerica Job ID: 720-32735-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 8260B/CA LUFTMS - 8260B/CA LUFT MS (Continued) <br /> Lab Sample ID: LCSD 720-84659/7 Client Sample ID: LCSD 720-84659/7 <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch: 84659 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Methylene Chloride 25.0 27.2 ug/L 109 73-147 1 20 <br /> trans-1,2-Dichloroethene 25.0 23.4 ug/L 94 75-131 0 20 <br /> cis-1,2-Dichloroethene 25.0 30.2 ug/L 121 70-130 0 20 <br /> Chloroform 25.0 28.2 ug/L 113 70-130 1 20 <br /> 1,1,1-Trichloroethane 25.0 28.4 ug/L 113 70-130 0 20 <br /> Carbon tetrachloride 25.0 27.2 ug/L 109 77-146 1 20 <br /> 1,2-Dichloroethane 25.0 27.5 ug/L 110 70-126 1 20 <br /> Trichloroethene 25.0 25.9 ug/L 104 70-130 0 20 <br /> 1,2-Dichloropropane 25.0 28A ug/L 114 70-130 1 20 <br /> Dichlorobromomethane 25.0 30.1 ug/L 120 70-130 2 20 <br /> trans-1,3-Dichloropropene 25.0 30.7 ug/L 123 83-140 2 20 <br /> cis-1,3-Dichloropropene 25.0 30.0 ug/L 120 88-137 1 20 <br /> 1,1,2-Trichloroethane 25.0 31.1 ug/L 124 82-128 2 20 <br /> Tetrachloroethene 25.0 22.8 ug/L 91 70-130 1 20 <br /> Chlorodibromomethane 25.0 26.6 ug/L 106 78-145 2 20 <br /> Chlorobenzene 25.0 24.6 ug/L 98 70-130 0 20 <br /> Bromoform 25.0 23.8 ug/L 95 68-136 3 20 El <br /> 1,1,2,2-Tetrachloroethane 25.0 27.8 ug/L 111 70-130 3 20 <br /> 1,3-Dichlorobenzene 25.0 24.3 ug/L 97 70-130 0 20 <br /> 1,4-Dichlorobenzene 25.0 22.5 ug/L 90 83-116 0 20 <br /> 1,2-Dichlorobenzene 25.0 24.7 ug/L 99 70-130 1 20 <br /> Chloromethane 25.0 20.5 ug/L 82 52-175 2 20 <br /> Bromomethane 25.0 23.2 ug/L 93 43-151 1 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 25.4 ug/L 101 42-162 0 20 <br /> ne <br /> EDB 25.0 30.0 ug/L 120 70-130 2 20 <br /> 1,2,4-Trichlorobenzene 25.0 24.6 ug/L 99 70-130 1 20 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 107 70-130 <br /> 4-Bromofluorobenzene 115 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 104 67-130 <br /> Lab Sample ID: MB 720-84681/5 Client Sample ID: MB 720-84681/5 <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch: 84681 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> 1,1-Dichloroethene ND 0.50 ug/L 01/13/1109:54 1 <br /> 1,1-Dichloroethane ND 0.50 ug/L 01/13/1109:54 1 <br /> Dichlorodifluoromethane ND 0.50 ug/L 01/13/1109:54 1 <br /> Vinyl chloride ND 0.50 ug/L 01/13/11 09:54 1 <br /> Chloroethane ND 1.0 ug/L 01/13/1109:54 1 <br /> Trichlorofluoromethane ND 1.0 ug/L 01/13/1109:54 1 <br /> Methylene Chloride ND 5.0 ug/L 01/13/11 09:54 1 <br /> trans-1,2-Dichloroethene ND 0.50 ug/L 01/13/1109:54 1 <br /> cis-1,2-Dichloroethene ND 0.50 ug/L 01/13/1109:54 1 <br /> Chloroform ND 1.0 ug/L 01/13/1109:54 1 <br /> 1,1,1-Trichloroethane ND 0.50 ug/L 01/13/11 09:54 1 <br /> Carbon tetrachloride ND 0.50 ug/L 01/13/11 09:54 1 <br /> TestAmerica San Francisco <br /> Page 103 of 142 04/20/2011 <br />