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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-20910-1 <br /> Matrix Spike/ Method: 8260B <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-53444 Preparation: 5030B <br /> MS Lab Sample ID: 720-21058-A-6 MS Analysis Batch: 720-53444 Instrument ID: Saturn 2K3 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: d:\data\200907\070609\SAA <br /> Dilution: 20 Initial Weight/Volume: 40 mL <br /> Date Analyzed: 07/06/2009 1958 Final Weight/Volume: 40 mL <br /> Date Prepared: 07/06/2009 1958 <br /> MSD Lab Sample ID: 720-21058-A-6 MSD Analysis Batch: 720-53444 Instrument ID: Saturn 2K3 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: d:\data\200907\070609\SA-W, <br /> Dilution: 20 Initial Weight/Volume: 40 mL <br /> Date Analyzed: 07/06/2009 2032 Final Weight/Volume: 40 mL <br /> Date Prepared: 07/06/2009 2032 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 113 114 60-140 1 20 <br /> 1,1-Dichloroethane 108 108 60-140 0 20 <br /> Dichlorodifluoromethane 101 97 38-140 3 20 <br /> Vinyl chloride 84 72 58-140 7 20 <br /> Chloroethane 112 110 51 -140 2 20 <br /> Trichlorofluoromethane 110 106 60-140 3 20 <br /> Methylene Chloride 116 111 40-140 5 20 <br /> trans-1,2-Dichloroethene 104 104 60-140 0 20 <br /> cis-1,2-Dichloroethene 109 107 60-140 0 20 <br /> Chloroform 106 99 60-140 7 20 <br /> 1,1,1-Trichloroethane 109 108 60-140 0 20 <br /> Carbon tetrachloride 106 109 60-140 2 20 <br /> 1,2-Dichloroethane 101 101 60-140 1 20 <br /> Trichloroethene 110 133 60-140 6 20 <br /> 1,2-Dichloropropane 104 104 60-140 0 20 <br /> Dichlorobromomethane 98 99 60-140 0 20 <br /> trans-1,3-Dichloropropene 90 92 60-140 2 20 <br /> cis-1,3-Dichloropropene 99 100 60-140 2 20 <br /> 1,1,2-Trichloroethane 100 102 60-140 1 20 <br /> Tetrachloroethene 110 110 60-140 1 20 <br /> Chlorodibromomethane 92 95 60-140 3 20 <br /> Chlorobenzene 109 111 60-140 3 20 <br /> Bromoform 102 100 56-140 3 20 <br /> 1,1,2,2-Tetrachloroethane 84 93 60-140 11 20 <br /> 1,3-Dichlorobenzene 99 98 60-140 1 20 <br /> 1,4-Dichlorobenzene 100 101 60-140 0 20 <br /> 1,2-Dichlorobenzene 110 116 60-140 5 20 <br /> Chloromethane 100 96 52-140 4 20 <br /> Bromomethane 51 88 23-140 53 20 F <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> TestAmerica San Francisco Page 22 of 25 <br />