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QC Sample Results C <br /> Client: ECM Consultants TestAmerica Job ID: 720-85751-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 82608 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCS 440-469721/6 Client Sample ID: Lab Control Sample <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 469721 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Dichlorobromomethane 25.0 24.1 ug/L 97 70-132 <br /> Bromoform 25.0 24.2 ug/L 97 60-148 <br /> Bromomethane 25.0 23.9 ug/L 95 64.139 <br /> Carbon tetrachloride 25.0 22.1 ug/L 88 60-150 <br /> Chlorobenzene 25.0 23.2 ug/L 93 70-130 <br /> Chloroethane 25.0 23.8 ug/L 95 64-135 <br /> Chloroform 25.0 22.8 ug/L 91 70-130 <br /> Chloromethane 25.0 20.9 ug/L 83 47-140 <br /> Chlorodibromomethane 25.0 24.3 ug/L 97 69-145 <br /> 1,2-Dichlorobenzene 25.0 23.1 ug/L 92 70-130 <br /> 1,3-Dichlorobenzene 25.0 22.8 ug/L 91 70-130 <br /> 1,4-Dichlorobenzene 25.0 23.0 ug/L 92 70-130 <br /> EDB 25.0 24.4 ug/L 98 70-130 <br /> Dichlorodifluoromethane 25.0 19.0 ug/L 76 29-150 <br /> 1,1-Dichloroethane 25.0 23.4 ug/L 93 64-130 ❑ <br /> 1,2-Dichloroethane 25.0 24.4 ug/L 97 57.138 <br /> 1,1-Dichloroethene 25.0 22.7 ug/L 91 70-130 <br /> cis-1,2-Dichloroethene 25.0 23.6 ug/L 95 70-133 <br /> trans-1,2-Dichloroethene 25.0 24.2 ug/L 97 70-130 <br /> 1,2-Dichloropropane 25.0 25.8 ug/L 103 67-130 <br /> cis-1,3-Dichloropropene 25.0 25.1 ug/L 100 70-133 <br /> trans-1,3-Dichloropropene 25.0 24.4 ug/L 98 70-132 <br /> Methylene Chloride 25.0 21.2 ug/L 85 52-130 <br /> 1,1,2,2-Tetrachloroethane 25.0 23.5 ug/L 94 63-130 <br /> Tetrachloroethene 25.0 22.9 ug/L 92 70-130 <br /> 1,2,4-Trichlorobenzene 25.0 23.0 ug/L 92 60-140 <br /> 1,1,1-Trichloroethane 25.0 22.9 ug/L 92 70-130 <br /> 1,1,2-Trichloroethane 25.0 24.5 ug/L 98 70-130 <br /> Trichloroethene 25.0 24.1 ug/L 96 70-130 <br /> Trichlorofluoromethane 25.0 23.4 ug/L 93 60-150 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 23.5 ug/L 94 60-140 <br /> ne <br /> Vinyl chloride 25.0 22.2 ug/L 89 59-133 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 102 80-128 <br /> 4-Bromofluorobenzene(Surr) 97 80-120 <br /> Dibromofluoromethane(Surr) 100 76-132 <br /> Lab Sample ID: LCSD 440-469721/7 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 469721 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Dichlorobromomethane 25.0 24.6 ug/L 98 70-132 2 20 <br /> Bromoform 25.0 25.2 ug/L 101 60-148 4 25 <br /> Bromomethane 25.0 23.9 ug/L 95 64-139 0 20 <br /> Carbon tetrachloride 25.0 22.6 ug/L 90 60-150 2 25 <br /> TestAmerica Pleasanton <br /> Page 47 of 81 4/20/2018 <br />