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QC Sample Results C <br /> Client: ECM Consultants TestAmerica Job ID: 720-85751-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 82608 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: 720-85751-21 MS Client Sample ID: M-34C <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 469877 L <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 102 80-128 <br /> 4-Bromofluorobenzene(Surr) 102 80-120 <br /> Dibromofluoromethane(Surr) 102 76-132 <br /> Lab Sample ID: 720-85751-21 MSD Client Sample ID: M-34C <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 469877 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Dichlorobromomethane ND 25.0 24.5 ug_/L 98 70-138 2 20 <br /> Bromoform ND 25.0 24.2 ug/L 97 59-150 4 25 <br /> Bromomethane ND 25.0 24.1 ug/L 96 62-131 2 25 <br /> Carbon tetrachloride ND 25.0 22.8 ug/L 91 60-150 3 25 <br /> Chlorobenzene ND 25.0 23.6 ug/L 94 70-130 1 20 <br /> Chloroethane ND 25.0 24.2 ug/L 97 68-130 2 25 ❑ <br /> Chloroform ND 25.0 23.4 ug/L 93 70-130 1 20 <br /> Chloromethane ND 25.0 21.1 ug/L 84 39-144 1 25 <br /> Chlorodibromomethane ND 25.0 24.4 ug/L 97 70-148 3 25 <br /> 1,2-Dichlorobenzene ND 25.0 23.9 ug/L 95 70-130 1 20 <br /> 1,3-Dichlorobenzene ND 25.0 23.4 ug/L 93 70-130 0 20 <br /> 1,4-Dichlorobenzene ND 25.0 23.5 ug/L 94 70-130 0 20 <br /> EDB ND 25.0 25.4 ug/L 102 70-131 5 25 <br /> Dichlorodifluoromethane ND 25.0 17.6 ug/L 71 25-142 8 30 <br /> 1,1-Dichloroethane ND 25.0 23.8 ug/L 95 65-130 1 20 <br /> 1,2-Dichloroethane ND 25.0 25.0 ug/L 100 56-146 4 20 <br /> 1,1-Dichloroethene ND 25.0 23.3 ug/L 93 70-130 3 20 <br /> cis-1,2-Dichloroethene ND 25.0 24.0 ug/L 96 70-130 1 20 <br /> trans-1,2-Dichloroethene ND 25.0 25.0 ug/L 100 70-130 4 20 <br /> 1,2-Dichloropropane ND 25.0 26.1 ug/L 104 69-130 3 20 <br /> cis-1,3-Dichloropropene ND 25.0 25.5 ug/L 102 70-133 2 20 <br /> trans-1,3-Dichloropropene ND 25.0 24.5 ug/L 98 70-138 5 25 <br /> Methylene Chloride ND 25.0 21.7 ug/L 87 52-130 3 20 <br /> 1,1,2,2-Tetrachloroethane ND 25.0 24.9 ug/L 100 63-130 8 30 <br /> Tetrachloroethene ND 25.0 24.1 ug/L 96 70-137 1 20 <br /> 1,2,4-Trichlorobenzene ND 25.0 23.1 ug/L 93 60-140 2 20 <br /> 1,1,1-Trichloroethane ND 25.0 23.1 ug/L 93 70-130 3 20 <br /> 1,1,2-Trichloroethane ND 25.0 25.3 ug/L 101 70-130 5 25 <br /> Trichloroethene ND 25.0 24.7 ug/L 99 70-130 0 20 <br /> Trichlorofluoromethane ND 25.0 23.9 ug/L 95 60-150 4 25 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 25.0 24.2 ug/L 97 60-140 3 20 <br /> ne <br /> Vinyl chloride ND 25.0 22.9 ug/L 91 50-137 4 30 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 103 80-128 <br /> 4-Bromofluorobenzene(Surr) 100 80-120 <br /> Dibromofluoromethane(Surr) 102 76-132 <br /> TestAmerica Pleasanton <br /> Page 55 of 81 4/20/2018 <br />