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QC Sample Results C <br /> Client: ECM Consultants TestAmerica Job ID: 720-87316-1 <br /> Project/Site: Nestle <br /> Method: 82608 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCS 720-247313/5 Client Sample ID: Lab Control Sample <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 247313 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> 1,1,2-Trichloroethane 25.0 27.2 ug/L 109 80-117 <br /> Tetrachloroethene 25.0 26.3 ug/L 105 81-130 <br /> Chlorodibromomethane 25.0 28.7 ug/L 115 77-133 <br /> Chlorobenzene 25.0 25.3 ug/L 101 76-116 <br /> Bromoform 25.0 25.6 ug/L 103 75-127 <br /> 1,1,2,2-Tetrachloroethane 25.0 25.2 ug/L 101 70-115 <br /> 1,3-Dichlorobenzene 25.0 25.8 ug/L 103 76-116 <br /> 1,4-Dichlorobenzene 25.0 25.3 ug/L 101 76-116 <br /> 1,2-Dichlorobenzene 25.0 24.4 ug/L 98 77-117 <br /> Chloromethane 25.0 19.3 ug/L 77 49-134 <br /> Bromomethane 25.0 21.6 ug/L 86 70-132 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 24.8 ug/L 99 70-133 <br /> ne <br /> EDB 25.0 26.6 ug/L 106 80-121 <br /> 1,2,4-Trichlorobenzene 25.0 26.2 ug/L 105 78-120 ❑ <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 90 70-130 <br /> 4-Bromofluorobenzene 83 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 92 72-130 <br /> Lab Sample ID: LCSD 720-247313/6 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 247313 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1-Dichloroethene 25.0 22.5 ug/L 90 69-119 0 20 <br /> 1,1-Dichloroethane 25.0 24.7 ug/L 99 77-119 2 20 <br /> Dichlorodifluoromethane 25.0 10.1 ug/L 41 21-150 10 20 <br /> Vinyl chloride 25.0 19.0 ug/L 76 58-138 4 20 <br /> Chloroethane 25.0 21.6 ug/L 87 70-131 1 20 <br /> Trichlorofluoromethane 25.0 22.1 ug/L 88 75-141 4 20 <br /> Methylene Chloride 25.0 23.5 ug/L 94 75-117 0 20 <br /> trans-1,2-Dichloroethene 25.0 24.4 ug/L 98 79-117 0 20 <br /> cis-1,2-Dichloroethene 25.0 27.2 ug/L 109 77-117 2 20 <br /> Chloroform 25.0 25.9 ug/L 103 82-119 1 20 <br /> 1,1,1-Trichloroethane 25.0 25.9 ug/L 104 74-130 1 20 <br /> Carbon tetrachloride 25.0 26.0 ug/L 104 72-142 1 20 <br /> 1,2-Dichloroethane 25.0 25.7 ug/L 103 73-122 3 20 <br /> Trichloroethene 25.0 25.5 ug/L 102 80-123 2 20 <br /> 1,2-Dichloropropane 25.0 25.8 ug/L 103 79-119 2 20 <br /> Dichlorobromomethane 25.0 26.3 ug/L 105 81-130 5 20 <br /> trans-1,3-Dichloropropene 25.0 27.6 ug/L 110 76-122 1 20 <br /> cis-1,3-Dichloropropene 25.0 26.3 ug/L 105 82-119 2 20 <br /> 1,1,2-Trichloroethane 25.0 26.4 ug/L 106 80-117 3 20 <br /> Tetrachloroethene 25.0 25.7 ug/L 103 81-130 2 20 <br /> Chlorodibromomethane 25.0 27.6 ug/L 110 77-133 4 20 <br /> Chlorobenzene 25.0 24.9 ug/L 100 76-116 1 20 <br /> TestAmerica Pleasanton <br /> Page 57 of 77 7/18/2018 <br />