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QC Sample Results C <br /> Client: ECM Consultants TestAmerica Job ID: 720-87315-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 82608 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: 720-87315-13 MSD Client Sample ID: RPS-1 <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 247273 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 93 70-130 <br /> 4-Bromofluorobenzene 91 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 95 72-130 <br /> i <br /> Method: 300.0 - Anions, Ion Chromatography <br /> Lab Sample ID: MB 720-247185/4 Client Sample ID: Method Blank <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 247185 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Nitrate as N ND 0.23 mg/L 07/03/18 17:23 1 <br /> Lab Sample ID: LCS 720-247185/5 Client Sample ID: Lab Control Sample <br /> Matrix: Water Prep Type: Total/NA ❑ <br /> Analysis Batch: 247185 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Nitrate as N 2.26 2.17 mg/L 96 90-110 <br /> Lab Sample ID: 720-87315-15 MS Client Sample ID: 7501 KIERNAN 2008 MID <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 247185 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Nitrate as N 2.7 22.6 25.1 mg/L 99 86--120 <br /> Lab Sample ID: 720-87315-15 MSD Client Sample ID: 7501 KIERNAN 2008 MID <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 247185 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Nitrate as N 2.7 22.6 25.1 mg/L 99 80-120 0 20 <br /> Method: 200.8 - Metals (ICP/MS) <br /> Lab Sample ID: MB 500-440135/1-A Client Sample ID: Method Blank <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 440442 Prep Batch: 440135 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Arsenic ND 1.0 ug/L 07/09/1810:15 07/10/1812:06 1 <br /> FLab Sample ID: LCS 500-440135/2-A Client Sample ID: Lab Control Sample <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 440442 Prep Batch: 440135 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Arsenic 100 100 ug/L 100 85-115 <br /> TestAmerica Pleasanton <br /> Page 33 of 52 7/18/2018 <br />