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LancasterAnalysis Report lop Laboratories Y p 2425 New Holland Pike PO Boot 12425 Lancaster PA 17605.2425•717 656 23oo Fax 717 656 2681•www lancasterlabs cont Page 8 of 9 Quality Control Summary Client: Name ChevronTexaco Group Number 877375 Reported 12/23/03 at 02 19 PM Surrogate Quality Control 4177747 100 101 103 98 4177748 101 100 105 98 4177749 100 101 104 99 4177750 100 101 103 99 4177751 100 102 103 100 4177752 100 101 103 98 4177753 100 102 103 99 4177754 99 100 104 99 Blank 100 99 104 97 LCS 99 99 104 98 Ms 101 101 104 98 MSD 100 101 104 98 Limits 81-120 82-112 85-112 83-113 Analysis Name BTEX+5 Oxygenates+ETOH Batch number P033441AA 4-Bromofluorobenzene Dibromofluoromethane 1,2-Dzchloroethane-d4 Toluene-de 4177733 101 102 105 99 4177734 100 98 103 96 4177735 100 100 103 97 4177736 100 100 104 98 4177737 99 100 104 98 4177739 100 101 104 97 4177740 100 101 104 97 4177741 99 100 104 99 4177742 100 102 103 97 4177743 100 101 104 98 4177744 100 100 103 97 4177755 98 99 105 99 4177756 100 100 103 97 4177757 99 100 103 97 Blank 100 100 104 97 103 98 100 LCS 100 Ms 100 100 104 95 MSD 99 101 104 98 Limits 81-120 82-112 85-112 B3-113 Analysis Name BTEX+5 Oxygenates+ETOH Batch number P033442AA 4-Bromofluorobenzene Dibromofluoromethc 1,2-Dichloroet:hane-d4 Toluene-d8 4177745 100 99 104 97 4177758 99 102 104 98 4177759 100 102 105 97 4177760 99 100 104 97 4177761 101 101 104 97 4177762 100 101 103 97 4177763 101 102 104 97 4177764 100 101 105 97 4177765 100 102 104 98 Blank 100 100 104 97 LCS 99 99 103 97 MS 99 fol 98 105 98 MSD 100 104 98 Limits 81-120 B2-112 85-112 83-113 "-Outside of specification (1) The result for one or both determinations was less than five times the LOQ (2) The background result was more than four times the spike added