ARCHIVED REPORTS_XR0003165 - Laserfiche WebLink

Home Browse Search

' M 111 M VERIFICATION LABORATORY AN, ISIS oxYMNATES TANK TANK TPH-G TPH-D BTX&.E CL HC TOTAL MTBE (MTBE, METALS PCB CONTENTS 8015 8015 8020 8010 LEAD 8020 TBA,DIPE, [CAP/ 8270 8260 8260 8260 8240 7420 8260 ETBE TAME) AAs or 5080 8260 7421 8260 LEADED GAS X X X X UNL GAS X X X DIESEL X X ' 14LEROSENE X X X UNK FUEL X X X X X OIL X X X CHLOR SOLVENTS X X X NONCHLOR X SOLVENTS X X W A STET USED OIL X X X X �( X X All analysts methods are the designated EPA methods described in EPA SW 846,Third Edition Those methods not found in SW 846 are specifically noted below Refer to the "SWRCB LUFT Field Manual",Appendix D (B),Table 3-5 on page A20 for minimum detection limits for motor vehicle fuel(gasoline and diesel) Refer to"Tri-Regional Board Staff Recommendations for Initial Evaluation and Investigation of UST's" for the waste and motor oil rtunimum detection limits Detection Limits that remain below the MCL,STLC or Alloy able Limit of the contanunant in question will be accepted, however laboratory shall utilize the most conservattre method 1 LABORATORY ANALYSES TERMINOLOGY TPH-G Total Petroleum Hydrocarbon,Gasoline,GC/f ID(5030)8015 mod or GUMS 8260 TPH-D Total Petroleum Hydrocarbon,Diesel,GC/FID(3550), 8015 mod or GC/MS 8260 BTX&E Benzene,Toluene,Xylcnc & Ethyl Benzene,GC/PID 8020 or GC/MS 8260 CL HC Chlorinated Hydrocarbon,GC/HSD 8010,GC/MS 8240 or 8260 TOTAL LEAD Total]cad,AA 7420, AA 7421 or ICP-AES 6010 OXYGENATES MTBE,ETBE,TAME,DIPE,&TBA GUMS 8260(For MTBE screen only you may use 8020) ' METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000 Metals Cadmium,Chromium ;11 and VI,Lead,Zinc and Nickel PCB Polychlorinated Biphenyls,GC/MS 8270 or 8080 GC-FID Gas Chromatography,F1amc Ionization Detection ,Method 3050 Acid digestion Method 3540 Soxhlet sample preparation Method 3550 Sonication sample preparation,extraction method Method 5030 Purge and trap sample preparation QA/QC Quality Assurance/Quality Control Nalco I'a avuld f,ilu 1110AWL detetltua of bu/cu,beii/me flee solvelas,111L to be used FUSILd Uplilaly LUIUIUflb att:litcft:ticd to liar-ked columns,a packed column may be used as a"first cut"with"dirty"samples or once the hydrocarbons have been characterized and proper QA/QC is followed For drinking water sources, EPA recommends that the 500 series for volatile organic should be used in preference to the 600 series because the detection limits arc lower and the QA/QC is better Samples exhibiting any level of heavy metal contamination may require further analysis EHD recommends holding those samples until digposal is indicated ;0 EH 23 046 (Revised 3115/02) Page 8