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TABLE II <br /> TCLP SAMPLING METHODS* <br /> Recommended Sampling Cartainers`, Preservation <br /> Techniques, and Holding Times <br /> Anst"ft Method Fluid Sediment and Soil Preservation Holding <br /> Time <br /> Volatile Organics: Two 40-ml volatile organic analysis vials One Boz,wide mouth glass Jar with Chill to 4°C 14 days <br /> -Appropriate TCLP methods fitted with Teflon septa (VOA vials) and Teflon septum, brass tube,or <br /> two 1-11ter amber glass botties with Teflon stainless steel tube <br /> septa <br /> • <br /> Semi-volatiN Organics: One 141ter amber glass bottle with Teflon One 8-oz.wide mouth glass)ar with Chill to 4°C 7 days <br /> -Appropriate TCLP methods septum Teflon septum, brass tube,or <br /> stainless steel tube <br /> TCLP metals One 14her polyethylene bottle One 8-0z.wide mouth glass jar with Chill to 4'C 180 days <br /> -Arsenic: 7080 Teflon septum <br /> -Barium: 8010 <br /> -Cadmium:8010 <br /> -Chromium:8010 <br /> -Lead: 7421 <br /> -Selenium:7740 <br /> Silver: 8010 <br /> Mercury.7470 One 141ler polyethylene bottle One"z.wide mouth glass Jar with Chill to 4°C 28 days <br /> Teflon septum,braes tube,or <br /> stainless steel tube <br /> Notes; •The TCLP cannot be used with analytical methods for total petroleum hydrocarbons (TPH) and total recoverable petroleum hydrocarbons (TRPH). <br /> + Additional sample volume may be needed for quality control samples and for each physical phase to be analyzed separately. • <br /> 28 <br />